In this study, biological synthesis of silver nanoparticles (AgNPs) using Senna auriculata flower extract for antibacterial activities was reported. The silver spectra compared to the plant extract show a rightward shift in AgNP peaks, indicating successful nanoparticle formation. The absorption band at 302 nm and the disappearance or shift of other peaks further confirm the synthesis.
View Article and Find Full Text PDFSpinel cobalt ferrite/hexagonal strontium hexaferrite (2CoFeO/SrFeSmLaO; = 0.2, 0.5, 1.
View Article and Find Full Text PDFMesopores silica nanotubes (MSNTs)-based chemical sensors for the rapid detection and of highly selective Fe ions have been prepared. The novel nanosensors were prepared via immobilization of 1,10-phenanthroline-5-amine (PA) and bathophenanthroline (BP) onto the MSNTs. The resultant PA and BP sensors display high sensitivity for detection the Fe ions in tap water, river water, sea water, two units in simple cycle power station, and biological samples.
View Article and Find Full Text PDFACS Omega
August 2021
In this study, we are interested in preparing Fe(III), Pd(II), and Cu(II) complexes from new thiazole derivatives. All syntheses were elaborately elucidated to estimate their molecular and structural formulae, which agreed with those of mononuclear complexes. The square-planer geometry of Pd(II) complex (MATYPd) was the starting point for its use as a heterocatalyst in preparing pyrazole-4-carbonitrile derivatives using ultrasonic irradiation through a facile one-pot reaction.
View Article and Find Full Text PDFAl Amar gold ore is rich in sulfides of base metals and is commercially applied for the production of copper concentrate via floatation and gold bullion by cyanidation of tailing. The current process flowsheet suffers from low gold recovery (∼60%) and loss of metals in the hazardous stockpiled residue. This work addresses these drawbacks by a newly experimental redesign of the process circuit.
View Article and Find Full Text PDFThis work presents the synthesis of carbon nanotubes (CNTs) inside titania nanotube (TNTs) templates by a catalyst-free chemical vapor deposition (CVD) approach as composite platforms for photocatalytic applications. The nanotubular structure of TNTs prepared by electrochemical anodization provides a unique platform to grow CNTs with precisely controlled geometric features. The formation mechanism of carbon nanotubes inside nanotubular titania without using metal catalysts is explored and explained.
View Article and Find Full Text PDFElectrochemically engineered nanoporous anodized aluminium oxide (AAO) prepared on aluminium (Al) foil by anodization process was employed as a platform for loading different forms of selenium (Se) in order to investigate their release behaviour and potential application for localized drug delivery targeting bone cancer. Several forms of Se including inorganic Se (HSeO), organic Se ((CH)Se), metallic Se, their chitosan composites, electrodeposited (ED) and chemical vapour deposited (CVD) Se were explored and combined with another model drug (indomethacin). Structural, drug-loading and in vitro drug-releasing characteristics of prepared Se-based drug delivery carriers were characterized by scanning electron microscopy (SEM), thermogravimetric analysis (TGA) and UV-visible spectroscopy (UV-Vis), respectively.
View Article and Find Full Text PDFA smart and reversibly photoswitchable membrane based on an azobenzene photo-switch containing peptides attached inside the pores of nanoporous anodic alumina membranes (NAAMs) is presented. The transport of molecules of interest across the photoswitchable peptide (PSP) functionalized NAAMs can be effectively controlled and manipulated as a function of the photostationary state of the azobenzene group in a PSP.
View Article and Find Full Text PDFAim/background: The methods of instruction in pharmacy education are crucial and meant to suit the professional development and encompass the advanced variety of services and functions provided by the pharmacists to serve individual patients. The aim of this study was to determine the students' opinions on the adopted and preferred methods of instruction in pharmacy colleges in Kingdom of Saudi Arabia.
Methods: Opinions of Saudi pharmacy students regarding the adopted methods of learning were measured using a pretested questionnaire combined with Likert-type scales.