Nowadays, it is necessary and challenging to prepare monolithic catalysts, which are ready for use, preventing the tedious and complicated integration procedure of the powder materials onto a porous substrate. Herein, CuO nanoparticles are successfully synthesized onto a porous Cu foam in one pot the surface oxidation, coordination and precipitation reactions in a NHOH and HCl solution, and the optimum synthesis conditions are a NH : HCl ratio of 1 : 0.9, oxidation temperature of 80 °C and time of 18 h.
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