In recent years, the wine industry has shifted towards plant-based fining agents for food safety reasons and consumer preferences. This study analysed the interaction of five plant fibers with red wine phenolic compounds to determinate their performance as fining agents. Chemical composition, polysaccharide profile, and physical properties were examined.
View Article and Find Full Text PDFThis bibliometric analysis provides the first overview of the literature on emerging contaminants in coastal waters. Bibexcel, Microsoft Excel, VOSviewer and the bibliometix R package software were used for bibliometric analysis and science mapping. 556 publications, published between 1986 and 2022, were retrieved from the Web of Science (WoS) database.
View Article and Find Full Text PDFIn this study, risk estimation based on sampling and subsampling uncertainty was performed for pesticide analysis in homogeneous spice products such as paprika. The results of the subsampling were also used to estimate the minimum weight necessary in subsampling to minimize overall uncertainty. The results show that subsampling has more uncertainty than sampling in the product due to high homogeneity in the manufacturer's batch.
View Article and Find Full Text PDFInt J Environ Res Public Health
September 2021
Human breast milk is the most complete foodstuff for infants but can also be a potential source of exposure to toxic chemicals. The aim of this study was to assess the levels of metal pollution in the breast milk of women living in agricultural and industrial/mining areas of the Region of Murcia (Spain) that are well known for their cases of environmental pollution. Human milk samples were collected from 50 mothers and inorganic contaminants were analyzed using inductively coupled plasma mass spectrometry (ICP-MS).
View Article and Find Full Text PDFNowadays, the techniques for the analysis of glycosidic precursors in grapes involve changes in the glycoside structure or it is necessary the use of very expensive analytical techniques. In this study, we describe for the first time an approach to analyse intact glycosidic aroma precursors in grapes by high-performance liquid chromatography with a diode array detector (HPLC-DAD), a simple and cheap analytical technique that could be used in wineries. Briefly, the skin of Muscat of Alexandria grapes was extracted using a microwave and purified using solid-phase extraction combining Oasis MCX and LiChrolut EN cartridges.
View Article and Find Full Text PDFFood Addit Contam Part A Chem Anal Control Expo Risk Assess
November 2020
A QuEChERS multi-residue GC-MS/MS method was developed for determining 160 pesticides in fresh edible snails. The method was validated according to the EU guidance SANTE/12682/2019. Twenty-seven different pesticides were quantified in the 824 samples analysed.
View Article and Find Full Text PDFThis work aims to provide a comprehensive study of the available research information on pesticide residues in honey through literature analysis. The research advancements within this research field from 1948 to 2019 are addressed using the Web of Science database. The results from the 685 articles analyzed indicate that this research field is in the focus of interest nowadays (Price index: 47.
View Article and Find Full Text PDFA bibliometric analysis based on the Web of Science© (WOS) database was performed on bioavailability of pesticides in vegetables, food or wine related studies published from inception to 2018. A total of 1202 articles were subjected to examination. The results reveal that yearly production of scientific articles increased steadily.
View Article and Find Full Text PDFIntroduction: The aims of this study were: (i) to provide a detailed description of movement and nonmovement behaviors objectively assessed over the complete 24-h period in a sample of older adults, and (ii) to analyze differences in these behaviors by sex, age, educational level, body mass index, self-rated health, and chronic conditions.
Methods: The sample comprised 607 high-functioning community-dwelling older adults (383 women), 65 to 92 yr, who participated in the IMPACT65+ study. Movement and nonmovement behaviors were assessed by the Intelligent Device for Energy Expenditure and Activity, which provide estimates on both temporal and spatial gait parameters, and identify specific functional activities on the basis of acceleration and position information.
Introduction: Physical activity and physical inactivity patterns can affect health status. In the elderly people, their study is relevant given the importance that they have on the morbidity and mortality.
Objective: To present preliminary data on activity and inactivity patterns of a sub-sample of older adults from the IMPACT65+ Study.
The interday reliability of the Intelligent Device for Energy Expenditure and Activity (IDEEA) has not been studied to date. The study purpose was to examine the interday variability and reliability on two consecutive days collected with the IDEEA, as well as to predict the number of days needed to provide a reliable estimate of several movement (walking and climbing stairs) and nonmovement (lying, reclining, and sitting) behaviors and standing in older adults. The sample included 126 older adults (74 women) who wore the IDEEA for 48 hr.
View Article and Find Full Text PDFObjectives: The aims of the present study were (i) to develop automated algorithms to identify the sleep period time in 24 h data from the Intelligent Device for Energy Expenditure and Activity (IDEEA) in older adults, and (ii) to analyze the agreement between these algorithms to identify the sleep period time as compared to self-reported data and expert visual analysis of accelerometer raw data.
Approach: This study comprised 50 participants, aged 65-85 years. Fourteen automated algorithms were developed.
The effects of six clarification agents [egg albumin, blood albumin, bentonite + gelatine, charcoal, polyvinylpolypyrrolidine (PVPP) and silica gel] on the removal of residues of three fungicides (famoxadone, fluquinconazole and trifloxystrobin) applied directly to a racked red wine, elaborated from Monastrell variety grapes from the D.O. Region of Jumilla (Murcia, Spain) were studied.
View Article and Find Full Text PDFAnn Agric Environ Med
October 2005
In the Mediterranean province of Murcia (SE Spain) around 610,000 hectares of land are devoted to agriculture and organochlorine insecticide use has been common in the region for many years. To investigate HCH and DDT (isomers and metabolites) residues, a total of 231 fat samples were taken from the general population and analyzed. Organochlorine residues were found in 63.
View Article and Find Full Text PDFThe effects of three fungicide residues (cyprodinil, fludioxonil, and pyrimethanil) on the aromatic composition (acids, alcohols, and esters) of Vitis vinifera white wines (var. Airén) inoculated with three Saccharomyces cerevisiae strains (syn. bayanus, cerevisiae, and syn.
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