Instrumented Cylindrical Punch Indentation of Solid Nitrogen at 30-40 K.

In support of NASA's Triton Hopper project, mechanical response data for solid nitrogen are needed for concept validation and development. Available mechanical properties data is sparse with only three known indentation measurements existing between 30 and 40 K. To generate more data, a custom instrumented hardness tester was developed to interface with a cryostat.

Nanomechanical testing technique for millimeter-sized and smaller molecular crystals.

Large crystals are used as a control for the development of a mounting and nanoindentation testing technique for millimeter-sized and smaller molecular crystals. Indentation techniques causing either only elastic or elastic-plastic deformation produce similar results in assessing elastic modulus, however, the elastic indents are susceptible to surface angle and roughness effects necessitating larger sample sizes for similar confidence bounds. Elastic-plastic indentations give the most accurate results and could be used to determine the different elastic constants for anisotropic materials by indenting different crystal faces, but not by rotating the indenter about its axis and indenting the same face in a different location.