Publications by authors named "Masseboeuf A"

Magnetic skyrmions are topological spin textures which are envisioned as nanometer scale information carriers in magnetic memory and logic devices. The recent demonstrations of room temperature skyrmions and their current induced manipulation in ultrathin films were first steps toward the realization of such devices. However, important challenges remain regarding the electrical detection and the low-power nucleation of skyrmions, which are required for the read and write operations.

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  • Researchers developed new types of probes made from all-graphenic carbon morphologies attached to individual carbon nanotubes, which may enhance scanning probe microscopy (SPM) techniques.
  • They tested three methods for mounting these probes, two involving focused ion/electron beams and one using an optical microscope, highlighting the pros and cons of each method.
  • Analysis showed the carbon cone structures were highly sensitive to ion and electron irradiation, likely due to many free graphene edges, suggesting that these carbon cones could outperform traditional probes like silicon or diamond in SPM applications.
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The metal-oxide-semiconductor (MOS) capacitor is one of the fundamental electrical components used in integrated circuits. While much effort is currently being made to integrate new dielectric or ferroelectric materials, capacitors of silicon dioxide on silicon remain the most prevalent. It is perhaps surprising therefore that the electric field within such a capacitor has never been measured, or mapped out, at the nanoscale.

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  • - The study involves creating graphene-based carbon micro/nano-cones using a chemical vapor deposition method on carbon nanotubes and examining them with advanced microscopy and modeling techniques.
  • - The results showed that the cones have a scroll-like texture, with parallel scroll turns and a common helicity vector, allowing for possible coherent stacking despite curvature-induced lattice shifts.
  • - A unique graphene termination defect, termed the "zip" defect, was identified at the cone apexes, leading to a low Raman band ratio, and the findings contributed to a chart categorizing various defects affecting graphene structures.
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Perpendicular shape anisotropy (PSA) offers a practical solution to downscale spin-transfer torque magnetoresistive random-access memory (STT-MRAM) beyond the sub-20 nm technology node while retaining thermal stability. However, our understanding of the thermomagnetic behavior of PSA-STT-MRAM is often indirect, relying on magnetoresistance measurements and micromagnetic modeling. Here, the magnetism of a NiFe PSA-STT-MRAM nanopillar is investigated using off-axis electron holography, providing spatially resolved magnetic information as a function of temperature.

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The fabrication of multi-gigabit magnetic random access memory (MRAM) chips requires the patterning of magnetic tunnel junctions at very small dimensions (sub-30 nm) and a very dense pitch. This remains a challenge due to the difficulty in etching magnetic tunnel junction stacks. We previously proposed a strategy to circumvent this problem by depositing the magnetic tunnel junction material on prepatterned metallic pillars, resulting in the junction being naturally shaped during deposition.

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  • Focused Electron Beam Induced Deposition (FEBID) offers a new method for creating magnetic tips used in Magnetic Force Microscopy (MFM), presenting advantages over traditional sputtering methods.
  • FEBID allows for the fabrication of sharp magnetic nanorods, with tips reaching diameters of about 10 nm, enhancing lateral resolution and enabling more precise interaction with samples.
  • The innovative tips can be tailored for different mechanical properties and even used in liquid environments, expanding research possibilities, particularly in studies of magnetic biological samples.
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One-dimensional (1D) nanostructures have been regarded as the most promising building blocks for nanoelectronics and nanocomposite material systems as well as for alternative energy applications. Although they result in confinement of a material, their properties and interactions with other nanostructures are still very much three-dimensional (3D) in nature. In this work, we present a novel method for quantitative determination of the 3D electromagnetic fields in and around 1D nanostructures using a single electron wave phase image, thereby eliminating the cumbersome acquisition of tomographic data.

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A newly developed carbon cone nanotip (CCnT) has been used as field emission cathode both in low voltage SEM (30 kV) electron source and high voltage TEM (200 kV) electron source. The results clearly show, for both technologies, an unprecedented stability of the emission and the probe current with almost no decay during 1h, as well as a very small noise (rms less than 0.5%) compared to standard sources which use tungsten tips as emitting cathode.

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We present the first demonstration of ultrafast laser-induced field emission and measurement of the energy distribution of electrons from a nanotip based on a carbon nanotube (CNT). Our experimental setup extends the studies performed on conventional tungsten or gold tips by using this new innovative tip. The carbon tip consists of concentric carbon layers in the shape of a cone, and has been previously studied as a very good candidate for cold field emission.

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  • The study focuses on the cold-field emission properties of carbon cone nanotips (CCnTs), using a transmission electron microscope (TEM) for in situ analysis.
  • The relationship between current and voltage was examined and analyzed with the Fowler-Nordheim (F-N) equation, while off-axis electron holography mapped the electric field around the nanotip.
  • Results indicated a local electric field of 2.55 V/nm at a tip-anode distance of 680 nm and a work function of 4.8±0.3 eV for the CCnT was determined.
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We develop the self-assembly of epitaxial submicrometer-sized face-centered-cubic (fcc) Co(111) dots using pulsed laser deposition. The dots display atomically flat facets, from which the ratios of surface and interface energies for fcc Co are deduced. Zero-field magnetic structures are investigated with magnetic force and Lorentz microscopies, revealing vortex-based flux-closure patterns.

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A micromagnetic study of epitaxial micron-sized iron dots is reported through the analysis of Fresnel contrast in Lorentz Microscopy. Their use is reviewed and developed through analysis of various magnetic structures in such dots. Simple Landau configuration is used to investigate various aspects of asymmetric Bloch domain walls.

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Dimensionality crossover is a classical topic in physics. Surprisingly, it has not been searched in micromagnetism, which deals with objects such as domain walls (2D) and vortices (1D). We predict by simulation a second-order transition between these two objects, with the wall length as the Landau parameter.

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Thin film alloys with perpendicular anisotropy were studied using Lorentz transmission electron microscopy (LTEM). This work focuses on the configuration of domain walls and demonstrates the suitability and accuracy of LTEM for the magnetic characterization of perpendicular magnetic anisotropy materials. Thin films of chemically ordered (L1(0)) FePd alloys were investigated by micro-magnetic modeling and LTEM phase retrieval approach.

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Off-axis electron holography was used to observe and quantify the magnetic microstructure of a perpendicular magnetic anisotropic (PMA) recording media. Thin foils of PMA materials exhibit an interesting up and down domain configuration. These domains are found to be very stable and were observed at the same time with their stray field, closing magnetic flux in the vacuum.

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While magnetic hysteresis usually considers magnetic domains, the switching of the core of magnetic vortices has recently become an active topic. We considered Bloch domain walls, which are known to display at the surface of thin films flux-closure features called Néel caps. We demonstrated the controlled switching of these caps under a magnetic field, occurring via the propagation of a surface vortex.

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One side effect of the immunomodulatory effect of interferon is the possible triggering or exacerbation of systemic or cutaneous sarcoidosis. We report two new cases and offer an exhaustive review of the literature. A 39-year-old man with type C chronic active hepatitis developed new respiratory symptoms and pulmonary infiltrates with hilar and mediastinal adenopathy after 7 months of treatment with pegylated interferon.

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