Transition metal oxides based anodes are facing crucial problems of capacity fading at long cycles and high rates due to electrode degradations. In this prospective, an effective strategy is employed to develop advanced electrode materials for lithium-ion batteries (LIBs). In the present work, a mesoporous CoO@CdS hybrid sructure is developed and investigated as anode for LiBs.
View Article and Find Full Text PDFBi-functional materials provide an opportunity for the development of high-performance devices. Up till now, bi-functional performance of NiCoO@SnSnanosheets is rarely investigated. In this work, NiCoO@SnSnanosheets were synthesized on carbon cloth by utilizing a simple hydrothermal technique.
View Article and Find Full Text PDFBiosensors (Basel)
November 2022
The development of a highly sensitive and selective non-enzymatic electrochemical biosensor for precise and accurate determination of multiple disease biomarkers has always been challenging and demanding. The synthesis of novel materials has provided opportunities to fabricate dependable biosensors. In this perspective, we have presented and discussed recent challenges and technological advancements in the development of non-enzymatic cholesterol electrochemical biosensors and recent research trends in the utilization of functional nanomaterials.
View Article and Find Full Text PDFThe detection of cholesterol is very crucial in clinical diagnosis for rapid and accurate monitoring of multiple disease-biomarkers. There is a great need for construction of a highly reliable and stable electrocatalyst for the efficient detection of cholesterol. In this work, mesoporous NiCoSnanoflakes of enhanced electrochemical properties are prepared through a facile hydrothermal approach.
View Article and Find Full Text PDFObjective To investigate the diagnostic accuracy of the placental thickness measured by ultrasound sonography test (USG) in detecting intrauterine growth restriction (IUGR) babies in the third trimester of pregnancy, keeping IUGR (by parameters using Hadlock) as the gold standard. Methods and materials This cross-sectional study was conducted at the radiology department of KRL Hospital from August 5, 2020, to October 25, 2021. Informed written consent was also obtained from each patient, and the hospital's ethical committee approved the study.
View Article and Find Full Text PDFTwo-dimensional (2D) transition-metal dichalcogenide materials show potential for use in alkali metal ion batteries owing to their remarkable physical and chemical properties. Nevertheless, the electrochemical energy storage performance is still impaired by the tendency of aggregation, volume, and morphological change during the conversion reaction and poor intrinsic conductivity. Until now, ultrathin molybdenum disulfide nanosheets with a metallic-phase structure on the inner surface of mesoporous hollow carbon spheres (M-MoS@HCS) have rarely been investigated as an anode for sodium-ion batteries.
View Article and Find Full Text PDFThe development of a reliable non-enzymatic multi-analyte biosensor is remained a great challenge for biomedical and industrial applications. In this prospective, rationally designed electrode materials having voltage switchable electrocatalytic properties are highly promising. Here, we report vanadium doped ZnO engineered nanostructures (ZnVO where 0 ≤ ≤ 0.
View Article and Find Full Text PDFThe synthesis of one-dimensional heterostructures having high dielectric constant and low dielectric loss has remained a great challenge. Until now, the dielectric performance of ZnO-ZnS heterostructures was scarcely investigated. In this work, large-scale ZnO-ZnS heterostructures were synthesized by employing the chemical vapor deposition method.
View Article and Find Full Text PDFThe development of a highly sensitive and selective non-enzymatic electrode catalyst for the detection of a target molecule was remained a great challenge. In this regard, bimetallic nanowires (BMNWs) are considered as promising electrode material for their fascinating physical/chemical properties superior to a single system. In this article, nickel cobalt (Ni -Co) BMNWs with tunable stoichiometry were prepared by a template assisted electrodeposition method and their catalytic performance was investigated for the detection of hydrogen peroxide (HO).
View Article and Find Full Text PDFA thin layer of gold nanoparticles (Au NPs) sputtered on cadmium sulfide quantum dots (CdS QDs) decorated anodic titanium dioxide nanotubes (TNTs) (Au/CdS QDs/TNTs) was fabricated and explored for the nonenzymatic detection of cholesterol and hydrogen peroxide (HO). Morphological studies of the sensor revealed the formation of uniform nanotubes decorated with a homogeneously dispersed CdS QDs and Au NPs layer. The electrochemical measurements showed an enhanced electrocatalytic performance with a fast electron transfer (∼2 s) between the redox centers of each analyte and electrode surface.
View Article and Find Full Text PDFUltralong VO nanobelts have been successfully synthesized by a facile hydrothermal oxidation route. Oxygen vacancies are generated in the VO nanobelts by annealing under N atmosphere at an elevated temperature. The microstructure and chemical composition of the pristine and annealed VO nanobelts are studied by different methods.
View Article and Find Full Text PDFNiCoO is a potential anode material for lithium ion battery due to its many advantages, such as high theoretical capacitance, low cost, and good electrochemical activity. In this study, mesoporous NiCoO double-hemisphere (3-5 μm) with high surface area (270.68 m·g) and excellent electrochemical performances has been synthesized through a facile precipitation method followed with thermal treatment process.
View Article and Find Full Text PDFMaterials (Basel)
November 2017
Zinc oxide (ZnO) nanostructures have been studied extensively in the past 20 years due to their novel electronic, photonic, mechanical and electrochemical properties. Recently, more attention has been paid to assemble nanoscale building blocks into three-dimensional (3D) complex hierarchical structures, which not only inherit the excellent properties of the single building blocks but also provide potential applications in the bottom-up fabrication of functional devices. This review article focuses on 3D ZnO hierarchical nanostructures, and summarizes major advances in the solution phase synthesis, applications in environment, and electrical/electrochemical devices.
View Article and Find Full Text PDFJ Nanosci Nanotechnol
March 2011
In this letter, effect of Pb-doping on the electrical and optical properties of the as grown ZnO nanowires (NWs) have been investigated. The microstructural investigations show that the Pb-dopant substituted into wurtzite ZnO nanowires without forming any secondary phase. The amount of contents and valence state of Pb ions has been investigated through energy dispersive spectroscopy and X-ray photospectroscopy.
View Article and Find Full Text PDFACS Appl Mater Interfaces
April 2011
Vertically oriented well-aligned Indium doped ZnO nanowires (NWs) have been successfully synthesized on Au-coated Zn substrate by controlled thermal evaporation. The effect of indium dopant on the optical and field-emission properties of these well-aligned ZnO NWs is investigated. The doped NWs are found to be single crystals grown along the c-axis.
View Article and Find Full Text PDFBackground: Papillon-Lefevre syndrome is a rare autosomal recessive disorder caused by cathepsin C gene mutation leading to the deficiency of cathepsin C enzymatic activity. The disease is characterized by palmoplantar hyperkeratosis, loss of deciduous and permanent teeth and increased susceptibility to infections. Onset of palmoplantar hyperkeratosis and periodontopathy is most commonly before the age of 4 years.
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