Addressing challenges with evaluating hydrogen-selective membrane performance by quadrupole mass spectrometry.

Hydrogen separation using nanostructured membranes has gained research attention because of its potential to produce high-purity hydrogen by separating gases at the molecular level. Quadrupole mass spectrometry (QMS) is one method to evaluate these membranes' effectiveness in separating hydrogen from gas mixtures. However, quantifying gases in a mixture with QMS is challenging, especially when heavier gas ions interfere with a light gas ion, resulting in lower quantification accuracy.

Visualization of individual emission sites on flat broad-area field emission cathodes.

We introduce a novel scanning projection field emission microscope (SPFEM) designed to study flat broad-area field emission cathodes. The instrument merges capabilities of measuring the electron field emission current from an individual emitting site and genuine projection of electrons onto a luminescent screen. This is achieved by an optimized shape of the anode probe having a 0.