Calcination of nanoparticles is always accompanied by undesired sintering. A calcination route preventing hard-agglomeration to bulk lumps, which is transferable to almost any kind of metal oxide nanoparticle, is developed by surrounding targeted nanoparticles by silica nanoparticles within a nanostructured microparticle. After calcination, the desired nanoparticles are regained as a monodisperse sol silica dissolution.
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