Determination of Phase Jumps in the Measurement of Phase Velocity of Samples Obeying a Frequency Power-Law Attenuation Coefficient Using Kramers-Kronig Relations.

Ultrasonic phase velocity spectroscopy is a very sensitive technique used in the measurement of material properties. In a phase velocity calculation, ambiguities can arise in the spectral phases, in the form of integer multiples of 2π rad, which, if not corrected, results in large errors. In this work, we propose a method for determining these ambiguities, more specifically, the number of 2π rad phase jumps, using the Kramers-Kronig relations, for samples exhibiting a frequency power-law attenuation coefficient.

Versatile Ultrasonic Spectrometer for Liquids With Practical Sample Handling by Using Standard Cuvettes.

This work describes the development and tests of a new ultrasonic spectrometer for liquids based on the use of commercial cuvettes for sample handling. The spectrometer operates in the frequency range from 20 to 80 MHz and gathers some important characteristics, which are its high thermal stability (better than 0.01 °C), by the use of Peltier cells, and practical sample handling with small volume (≤3 ml) samples placed inside cuvettes which can be easily removed from the spectrometer, cleaned/sterilized, or simply discarded.