In this work, MnO/NiO nanocomposite electrode materials have been synthesized by a cost-effective hydrothermal method. The effect of the concentrations (0, 1, 3, 5, and 7 wt%) of NiO nanoparticles on the surface morphology, structural properties, and electrochemical performance of the nanocomposites was characterized by different characterization techniques. The scanning electron micrographs (SEM) reveal that the as-prepared NiO nanoparticles are well connected and stuck with the MnO nanowires.
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