In this work, Au/BiO was synthesized by loading Au nanoparticles (NPs) onto β-BiO by a simple solution reduction method. β-BiO was synthesized by a precipitation-thermal decomposition procedure, which results in significantly improved SERS detection limits down to 10 M for methylene blue (MB) and 10 M for methyl orange (MO) as probe molecules, comparable to those reported for the best semiconductor SERS substrates. In particular, further deposition of Au NPs (5.
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