Monitoring low levels of ammonia in chloraminated water can be challenging but is important for effectively managing potable water disinfection. The lower the concentration of free ammonia that can be determined, the tighter the control at the disinfection point, which supports better maintenance of chloramine residuals in the distribution system. In this study a micro-distillation technique was used to selectively separate ammonia into a boric acid solution allowing determination by conductance (i.
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