Publications by authors named "Kungumadevi L"

In this work, we have focused on the preparation of copper hexacyanoferrate/boron doped rGO composites (abbreviated as CuHCF/B-rGO) by employing simple co-precipitation technique subsequently processed with ultrasonication method. The XRD spectra confirmed the existence of the cubic structure of copper hexacyanoferrate with high crystalline peaks. The prepared nanocomposite morphology was evaluated by scanning electron microscopy (SEM), and confirmed CuHCF nanoparticles formation with flake-like and wrinkled sheets.

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In this study, the pristine MgO, MgO/CNT and Ni-MgO/CNT nanocomposites were processed using the impregnation and chemical vapor deposition methods and analyzed for hydrogen evolution reaction (HER) using the electrochemical water splitting process. Furthermore, the effect of nickel on the deposited carbon was systematically elaborated in this study. The highly conductive carbon nanotubes (CNTs) deposited on the metal surface of the Ni-MgO nanocomposite heterostructure provides a robust stability and superior electrocatalytic activity.

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Photocatalysts based on semiconducting chalcogenides due to their adaptable physio-chemical characteristics are attracting attention. In this work, Bi-doped PbS (henceforth PbS:Bi) was prepared using a straightforward chemical precipitation approach, and the influence of γ-irradiation on PbS's photocatalytic ability was investigated. Synthesized samples were confirmed structurally and chemically.

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Article Synopsis
  • * Characterization methods like X-ray diffraction and electron microscopy revealed that gamma-irradiation increased the optical bandgap of PbS from 1.95 eV to 2.45 eV.
  • * The gamma-irradiated PbCuSrS sample showed significant photocatalytic performance, achieving 74.02% degradation of methylene blue dye in 160 minutes, along with 69.4% stability after three usage cycles.
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Conversion and reducing agent (NaBH) effect on zero valent iron into FeO nanoparticles with diverse molar ratios of reducing agent was produced through chemical reduction technique. The structural, optical, vibrational analyses were executed via XRD, UV-Vis, Raman, and FT-IR analysis. The crystallite size obtained were 35 nm, 27 nm, and 18 nm for Fe:NaBH (1:1), Fe:NaBH (1:2) and Fe:NaBH (1:3).

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Herein, we reported the synthesis of BiOX (X = Cl, Br) with different grinding time like 15 min and 30 min to analyze the evolution of physiochemical properties and the morphological evolution. The structural, optical, vibrational properties were examined by standard characterization studies. The formation of bismuth oxyhalides were confirmed by XRD and Raman studies.

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Nanotechnology has undergone significant development in recent years, particularly in the fabrication of sensors with a wide range of applications. The backbone of nanotechnology is nanostructures, which are determined on a nanoscale. Nanoparticles are abundant throughout the universe and are thought to be essential building components in the process of planet creation.

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