A multiple channel-type concentric grid nebulizer (m-CGrid) was developed for realizing efficient online standard addition in inductively coupled plasma optical emission spectrometry (ICP-OES) without premixing of liquids before nebulization. The m-CGrid can nebulize two independent liquids without premixing due to a unique structure, having two independent liquid-flow capillaries inside a single nozzle and a grid screen (over 350 mesh per inch) placed on the hole of the nozzle. The grid acts as both a flow damper and sieve; two liquids are well-mixed with a gas flow in a small space just before the grid screen, and the mixture breaks up into small droplets by passing through the grid.
View Article and Find Full Text PDFA method was established for the quantitative analysis of the elements (Cu, Ag, Pb, and Sn) in solder samples by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS), with Sn-based matrix matched standard solutions for defining the calibration curves. It was found that chloride-ion presented in commercially available Sn standard solution resulted in a precipitation of AgCl and caused the deterioration of the linearity of the calibration curve for Ag. Therefore, a laboratory-made chloride-free Sn solution was used to prepare Sn matrix matched standard solutions so as to ensure the stability of the elements including Ag.
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