Analysis of Acetylated Hyaluronic Acid in Moisturizing Lotion and Milk Lotion by HPLC with Fluorescence Detection.

We developed a simple and sensitive analytical HPLC method for the determination of acetylated hyaluronic acid (AcHA) in moisturizing and milk lotions. AcHA with different molecular weights was separated as a single peak using a C4 column and detected through post-column derivatization using 2-cyanoacetamide. The limits of detection and quantification were 60 and 200 ng, respectively.

Simultaneous measurement of specific heat and thermal conductivity in pulsed magnetic fields.

We report an experimental setup for simultaneously measuring specific heat and thermal conductivity in feedback-controlled pulsed magnetic fields of 50 ms duration at cryogenic temperatures. A stabilized magnetic field pulse obtained by the feedback control, which dramatically improves the thermal stability of the setup and sample, is used in combination with the flash method to obtain absolute values of thermal properties up to 37.2 T in the 22-16 K temperature range.

Isolation and structural characterization of bioactive glycosaminoglycans from the green-lipped mussel Perna canaliculus.

Chondroitin sulfate (CS) and heparan sulfate (HS) are sulfated glycosaminoglycan (GAG) chains that consist of repeating disaccharide units composed of hexosamine and hexuronic acid. GAG chains exhibit diverse bioactivities in a structure-specific manner. Marine invertebrates are a rich source of highly sulfated and rare structures of GAG chains.

Homemade-HEMT-based transimpedance amplifier for high-resolution shot-noise measurements.

We report a cryogenic transimpedance amplifier (TA) suitable for cross-correlation current-noise measurements. The TA comprises homemade high-electron-mobility transistors with high transconductance and low noise characteristics, fabricated in an AlGaAs/GaAs heterostructure. The low input-referred noise and wide frequency band of the TA lead to a high resolution in current-noise measurements.

Laser-Beam-Patterned Topological Insulating States on Thin Semiconducting MoS_{2}.

Identifying the two-dimensional (2D) topological insulating (TI) state in new materials and its control are crucial aspects towards the development of voltage-controlled spintronic devices with low-power dissipation. Members of the 2D transition metal dichalcogenides have been recently predicted and experimentally reported as a new class of 2D TI materials, but in most cases edge conduction seems fragile and limited to the monolayer phase fabricated on specified substrates. Here, we realize the controlled patterning of the 1T^{'} phase embedded into the 2H phase of thin semiconducting molybdenum-disulfide by laser beam irradiation.

Strain-induced spontaneous Hall effect in an epitaxial thin film of a Luttinger semimetal.

Pyrochlore iridates have provided a plethora of novel phenomena owing to the combination of topology and correlation. Among them, much attention has been paid to [Formula: see text], as it is known as a Luttinger semimetal characterized by quadratic band touching at the Brillouin zone center, suggesting that the topology of its electronic states can be tuned by a moderate lattice strain and external magnetic field. Here, we report that our epitaxial [Formula: see text] thin films grown by solid-state epitaxy exhibit a spontaneous Hall effect that persists up to 50 K without having spontaneous magnetization within our experimental accuracy.

Evidence for Spin-Triplet Electron Pairing in the Proximity-Induced Superconducting State of an Fe-Doped InAs Semiconductor.

We provide evidence for spin-triplet electron pairing in proximity-induced superconductivity in a ferromagnetic semiconductor (In,Fe)As. As discovered in half-metallic materials, an extraordinarily long proximity range is observed. More surprising is a very strong concentration of supercurrent to the edges of the superconducting region, which is deduced from the extremely persistent oscillation of the critical current vs magnetic field.

Uncertainty in Young Adult Survivors of Childhood and Adolescent Cancer with Lower-Extremity Bone Tumors in Japan.

Childhood and adolescent survivors of cancerous lower-extremity bone tumors may be at unique risk of uncertainty about their future because of their specific cancer and/or physical disabilities secondary to treatment. This study aimed at clarifying survivors' uncertainty and related factors, including physical functioning, limb pain, and management of affected limbs. Self-administered questionnaires were distributed at two cancer hospitals in Japan.

Evidence for a quantum spin Hall phase in graphene decorated with BiTe nanoparticles.

Realization of the quantum spin Hall effect in graphene devices has remained an outstanding challenge dating back to the inception of the field of topological insulators. Graphene's exceptionally weak spin-orbit coupling-stemming from carbon's low mass-poses the primary obstacle. We experimentally and theoretically study artificially enhanced spin-orbit coupling in graphene via random decoration with dilute BiTe nanoparticles.

Conductance fluctuations in InAs quantum wells possibly driven by Zitterbewegung.

The highly successful Dirac equation predicts peculiar phenomena such as Klein tunnelling and Zitterbewegung (ZB) of electrons. From its conception by Erwin Schrödinger, ZB has been considered key in understanding relativistic quantum mechanics. However, observing the ZB of electrons has proved difficult, and instead various emulations of the phenomenon have been proposed producing several successes.

Gate-Tunable Atomically Thin Lateral MoS2 Schottky Junction Patterned by Electron Beam.

Among atomically thin two-dimensional (2D) materials, molybdenum disulfide (MoS2) is attracting considerable attention because of its direct bandgap in the 2H-semiconducting phase. On the other hand, a 1T-metallic phase has been revealed, bringing complementary application. Recently, thanks to top-down fabrication using electron beam (EB) irradiation techniques, in-plane 1T-metal/2H-semiconductor lateral (Schottky) MoS2 junctions were demonstrated, opening a path toward the co-integration of active and passive two-dimensional devices.

Adiabatic measurements of magneto-caloric effects in pulsed high magnetic fields up to 55 T.

Magneto-caloric effects (MCEs) measurement system in adiabatic condition is proposed to investigate the thermodynamic properties in pulsed magnetic fields up to 55 T. With taking the advantage of the fast field-sweep rate in pulsed field, adiabatic measurements of MCEs were carried out at various temperatures. To obtain the prompt response of the thermometer in the pulsed field, a thin film thermometer is grown directly on the sample surfaces.

Brief hypo-osmotic shock causes test cell death, prevents neurula rotation, and disrupts left-right asymmetry in Ciona intestinalis.

Ascidian Ciona intestinalis tadpole larvae exhibit left-right asymmetry. The photoreceptors are situated on the right side of the sensory vesicle, and the tail curls along the left side of the trunk within the chorion. In tailbud embryos, the Ci-pitx gene is expressed in the left-side epidermis.

The transition of adult patients with childhood-onset chronic diseases from pediatric to adult healthcare systems: a survey of the perceptions of Japanese pediatricians and child health nurses.

Background: Advances in medical science have enabled many children with chronic diseases to survive to adulthood. The transition of adult patients with childhood-onset chronic diseases from pediatric to adult healthcare systems has received attention in Europe and the United States. We conducted a questionnaire survey among 41 pediatricians at pediatric hospitals and 24 nurses specializing in adolescent care to compare the perception of transition of care from pediatric to adult healthcare services for such patients.

Temperature-dependent screening of the edge state around antidots in the quantum Hall regime.

The Aharonov-Bohm effect in a small array of antidots with a large aspect ratio is investigated in the quantum Hall regime. The evolution with temperature of the Aharonov-Bohm oscillations in the magnetic field versus gate voltage (B-V_{g}) plane reveals the temperature dependence of the screening. The self-consistently screened potential of the compressible band surrounding an antidot is observed to gain a progressively steeper slope with increasing temperature.

Quantum interference in radial heterostructure nanowires.

Core/shell heterostructure nanowires are one of the most interesting mesoscopic systems potentially suitable for the study of quantum interference phenomena. Here, we report on experimental observations of both the Aharonov-Bohm (h/e) and the Altshuler-Aronov-Spivak (h/2e) oscillations in radial core/shell (In2O3/InOx) heterostructure nanowires. For a long channel device with a length-to-width ratio of about 33, the magnetoresistance curves at low temperatures exhibited a crossover from low-field h/2e oscillation to high-field h/ e oscillation.

Observation of the Fano-Kondo antiresonance in a quantum wire with a side-coupled quantum dot.

We have observed the Fano-Kondo antiresonance in a quantum wire with a side-coupled quantum dot. In a weak coupling regime, dips due to the Fano effect appeared. As the coupling strength increased, conductance in the regions between the dips decreased alternately.

Observation of "partial coherence" in an Aharonov-Bohm interferometer with a quantum dot.

We report experiments on the interference through spin states of electrons in a quantum dot (QD) embedded in an Aharonov-Bohm (AB) interferometer. We have picked up a spin-pair state, for which the environmental conditions are ideally similar. The AB amplitude is traced in a range of gate voltage that covers the pair.

Competition and binding of arginine, imidazole, and aminoguanidine to endothelial nitric oxide synthase: aminoguanidine is a poor model for substrate, intermediate, and arginine analog inhibitor binding.

The oxygenase domains of nitric oxide synthases are unusual in that they contain at least three ligand binding sites; these correspond to the axial heme ligand position, the substrate binding site, and the pterin binding site. Ligands can occupy portions of a site or extend into regions of adjacent sites. Depending on the size, shape, and binding mode of ligands to these positions, cooperative and anticooperative interactions mediated conformationally and by binding domain overlap can be observed.

Tuning of the Fano effect through a quantum dot in an Aharonov-Bohm interferometer.

The Fano effect, which arises from an interference between a localized state and the continuum, reveals a fundamental aspect of quantum mechanics. We have realized a tunable Fano system in a quantum dot (QD) in an Aharonov-Bohm interferometer, which is the first convincing demonstration of this effect in mesoscopic systems. With the aid of the continuum, the localized state inside the QD acquires itinerancy over the system even in the Coulomb blockade.

[Three orthodontic cases with temporomandibular joint sounds].

Three orthodontically treated cases with sounds of the temporomandibular joint are presented. Case 1: Eight months after [formula: see text] extraction, bilateral TMJ sounds were noticed. The patient had a history of pre-orthodontic TMJ sounds and locking.