A chromatography-like propagation of water through the material bed was observed while performing supercritical fluid extraction of aroma plants having high moisture content. While parts of raw material bed placed at the inlet of the extraction vessel get dried after appropriate extraction time, the parts closer to the outlet not only stay wet but, in fact, gain more moisture than initial raw material. Presumably, water and other extractables with limited solubility in supercritical CO, get re-adsorbed onto the plant material surface along the extraction column and then desorbed further on.
View Article and Find Full Text PDFAn approach for polymer-carbon nanotube (CNT) composite preparation is proposed based on a two-step supercritical fluid treatment. The first step, rapid expansion of a suspension (RESS) of CNTs in supercritical carbon dioxide, is used to de-bundle CNTs in order to simplify their mixing with polymer in solution. The ability of RESS pre-treatment to de-bundle CNTs and to cause significant bulk volume expansion is demonstrated.
View Article and Find Full Text PDFVestn Otorinolaringol
July 2021
The features of impedance audiometry with a 226 Hz probe frequency in newborns and children in the first months of life after acute otitis media were analyzed. The age dynamics of tympanograms in children in the first year of life is determined.
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