The alumina and zirconia surfaces were pretreated with chemical etching using alkaline mixtures of ammonia, hydrogen peroxide and sodium hydroxide, and followed with application of the powder layer of Ca-deficient hydroxyapatite (CDH). The influence of etching bath conditions time and concentration on surface development, chemical composition and morphology of medicinal ceramic powders were studied. The following analyses were performed: morphology (scanning electron microscopy), phase composition (X-ray diffraction analysis), changes in binding interactions and chemical composition (FT-Infrared and Energy dispersive spectroscopies).
View Article and Find Full Text PDFPurpose: This paper is focused on the works concerning preparation of zirconium oxide ceramic blocks recommended for CAD/CAM systems used in prosthetic dentistry for manufacturing fixed prosthetic restorations.
Methods: Zirconium-yttrium-magnesium mixed ceramic oxides were prepared by sol-gel method via hydrolysis and condensation of zirconium alkoxide precursor (zirconium (IV) propoxide) with yttrium and magnesium nitrates diluted in 2-propanol. The aim of this work was to obtain 2% mol yttria-stabilized zirconia ceramic powders with magnesium as an additional tetragonal ZrO2 phase stabilizer in amount between 2÷6% mol (with 2% variable).
Mater Sci Eng C Mater Biol Appl
January 2010
The aim of the study was to fabricate a biodegradable bio-composite using only natural biological precursors for both composite components, i.e., for a support and for a filler.
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