The accumulation of small doses of hydrogen peroxide (HO) into food can cause many diseases in the human body, and it is urgent to develop efficient detection methods of HO. Herein, the hierarchical structure composite of NiCo-LDH nanosheets crosslinked NiMoO nanorods was grown in situ on carbon cloth (NiMoO NRs@NiCo-LDH NSs/CC) by micro-plasma assisted hydrothermal method. Thanks to the synergistic effect of three metals and (NiMoO NRs@NiCo-LDH NSs/CC) provided by nanorods/nanosheets hierarchical structure, NiMoO NRs@NiCo-LDH NSs/CC exposes more active sites and achieves rapid electron transfer.
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