Publications by authors named "Jose Fernando Solanilla-Duque"

Biopolymers used to mitigate the environmental impact needed establish biodegradation percentage. The thermal and structural changes of two plastic materials, a flexible film based on cassava starch - Poly(lactic acid) (PLA) and a semi-rigid cassava flour-stay cellulose fique fiber, were evaluated biodegradation under ISO 4855-1 standard. The tests were carried out for four weeks at constant temperature and flow of 58 °C ± 2 °C and 250 mL/h, using a mature compost as inoculum.

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The growing popularity of nutrient-rich foods, among which is quinoa, is due to the increasing demand for healthier choices. Oils and hydrolyzed proteins from these foods may help prevent various health issues. The objective of this work was to perform extraction from the endosperm of the grain from high-protein quinoa flour by physical means a differential abrasive milling process and extracting the oil using an automatic auger extractor at 160°C, as well as characterizing extracted oil.

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Article Synopsis
  • * The sheaths underwent a shredding and steam explosion process, enhancing fiber properties while the sap was filtered and evaporated, suggesting improved mechanical qualities from the treated fibers compared to their raw state.
  • * FT-IR and TGA analyses revealed varying thermal stabilities and properties among the sap, starch, and fibers, with yarns produced showing differences based on their processing methods, highlighting the potential for value-added use of plantain
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One of the activities most representative of the agricultural sector in Colombia is the production of biodegradable fique fiber. The efficiency of the defiberization process of the fique leaves is very low since a mere 4% of the total weight of the leaf () is used and marketed. The remaining 96%, composed of fique juice and bagasse, is considered to be waste and discarded, impacting the environment.

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The interfacial and foaming properties of two conjugates obtained by Maillard reaction was determinate, at heating times of 36 and 60 h. The effect of covalent interaction between β-lactoglobulin (β-Lg) and two dextran molecular weights (10 and 20 kDa) were evaluated at pH 7 and pH 5, establishing protein controls, mixed systems, and mixing controls for each system. At pH 7, the first conjugate showed an increase in surface activity, while the other showed an opposite effect on the glycosylation process.

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The indiscriminate accumulation of plastic waste has prompted research that leads to obtaining biobased materials. The research aim was to evaluate the effect of incorporating fique bagasse microparticles (FBM) in a cassava starch-based foamed material. First, the FBM extraction conditions were established by acid hydrolysis, for which the effect of acid concentration (5, 10 and 15% HSO), temperature (70, 80 and 90 °C) and extraction time (3, 5 and 7 h) on particle size, functional groups, color, and thermal properties was evaluated.

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Ulomoides dermestoides (UL) are macroinvertebrates insects belonging to Tenebrionidae Coleopteran family. They were used to hasten, in five days, the biodegradation-mineralization of thermoplastic starch (TPS)-poly(lactic acid) (PLA) films, otherwise biodegradable under composting conditions. After the contact of TPS-PLA film with UL for five days, TPS was metabolized and PLA was hydrolysed, as evidenced by decreasing of hydroxyl and carbonyl group peaks intensity by FTIR spectra, increasing of 13% of PLA crystallinity by DSC thermograms, reduction of PLA and TPS thermal stability by TGA analysis; faecal residues evidenced two glass transition temperature T, at 33 °C and 57 °C, associated with depolymerized TPS and PLA, respectively.

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Contamination caused by the accumulation of petrochemical-based plastics has reached worrying magnitudes and led to the development of biopolymers as an option to mitigate the problem. This work thus presents a bibliometric analysis of all that concerns the development of such bionanocomposite materials, using ScientoPy and SciMAT software to establish associations between the number of published documents, countries, institutions and most relevant topics. The bionanocomposites topic was found to throw up the biggest number of documents associated (2008) with the different types of raw materials and methods used to obtain nanoparticles and their combination with biopolymeric materials, the result known as a "bionancomposite*".

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Article Synopsis
  • The study analyzed the nutrient composition, minerals, polyphenolic compounds, and antioxidant properties of green bean, mesquite, and pea flours.
  • Different combinations of these legume flours with wheat flour were tested for making bread, focusing on their effects on composition, color, volume, and functional properties.
  • Mesquite flour stood out for its high fiber and polyphenol content, while pea and green bean flours boosted protein levels, suggesting these legume flours can enhance the nutrition of baked products.
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TPS/MA/PLA is a blend of thermoplastic starch (TPS) and polylactic acid (PLA) compatibilized by maleic anhydride (MA) that can be a substitute for petro-based plastics in certain applications. At the end of its life, this material must be properly disposed in treatment systems such as composting or anaerobic digestion. The biodegradability of TPS/MA/PLA, PLA, TPS and the non-compatible mixture (TPS/PLA) was evaluated in a slurry thermophilic anaerobic digestion system (STAD) according to ISO 13975-2012 standard.

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Polylactic acid (PLA) and starch are compounds used in the manufacture of packaging to replace petroleum products as biodegradable and environmentally friendly materials. This study evaluated the structure and surface of a film manufactured by extrusion from cassava starch and PLA, which underwent a biodegradation process under compost conditions following the guidelines of ISO 4855-2:2007. Samples were taken every week for one month to perform Fourier Transform Infrared Spectroscopy (FT-IR) tests to identify functional groups on film, and High-Resolution Optical Microscopy (HROM) and Scanning Electron Microscopy (SEM) tests, from these techniques Structural changes in the film were evidenced.

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