Publications by authors named "Jolanta Was-Gubala"

Some of the most common microtraces that are currently collected at crime scenes are fragments of single fibers. The perpetrator leaves them at a crime scene or takes them away, for example, on their clothing or body. In turn, the microscopic dimensions of such traces mean that the perpetrator does not notice them and therefore usually does not take action to remove them.

View Article and Find Full Text PDF

The purpose of this work was to assess the usefulness of thin layer chromatography (TLC) for discriminating single cotton fibres dyed with red reactive dyes. An effective enzymatic extraction procedure with the use of cellulase for the red reactively-dyed cotton fibres was developed and used for the discrimination of fibres derived from 21 garments purchased commercially. Discrimination of the fibres relied on the separation of the extracted dyes by thin layer chromatography (TLC).

View Article and Find Full Text PDF

In forensic laboratories, the most commonly analyzed microtraces are microscopic fragments of single fibers. One of the main goals of the examination of fragments of fibers a few millimeters long is to determine their characteristic physicochemical properties and compare them with fibers originating from a known source (e.g.

View Article and Find Full Text PDF

The main purposes of this study was to assess the usefulness of microspectrophotometry (MSP), both in the ultraviolet (UV) and visible (Vis) range for discriminating single cotton fibres dyed with reactive dyes coming from the same manufacturer, as well as the possibility of evaluation of the concentration of dye in an examine fibre. This study utilised woven cotton fabrics dyed with different concentrations of one-compound reactive dyes with the commercial name Cibacron® (at present Novacron®) as the focus of the MSP analysis. The spectra were recorded in the UV-Vis range between 200 and 800nm, in transmission mode.

View Article and Find Full Text PDF

Presented in this paper is an assessment of the applicability of Raman spectroscopy and microspectrophotometry (MSP) in visible and ultraviolet light (UV-Vis) in the examination of textile fibers dyed with mixtures of synthetic dyes. Fragments of single polyester fibers, stained with ternary mixtures of disperse dyes in small mass concentrations, and fragments of single cotton fibers, dyed with binary or ternary mixtures of reactive dyes, were subjected to the study. Three types of excitation sources, 514, 633, and 785 nm, were used during Raman examinations, while the MSP study was conducted in the 200 to 800 nm range.

View Article and Find Full Text PDF

The aim of this study was to assess colour variations that occur in several types of textiles and their constituent fibres, resulting from the long-term influence of various laundry detergents. A 14-day experiment was conducted using blue, red and grey/black cotton, wool, acrylic and polyester textiles. The spectrophotometric measurement of colour changes in fabric samples and test solutions, as well as the microspectrophotometric analysis of colour changes in single fibres were described.

View Article and Find Full Text PDF

The aim of this study was to assess colour changes that occur in several types of commonly available textiles as a result of the long-term effects of various popularly used laundry detergents. A 14 day experiment was conducted using blue, red and grey/black cotton, wool, acrylic and polyester textiles. Colour changes were evaluated through the visual comparison of the colour of the textile samples against that of the untreated (control) material.

View Article and Find Full Text PDF

The report presents the results of identification of garments and other textile products, as well as various materials, e.g. fragments of metals, wood slivers and chemical substances found in the coffin by the body of General Władysław Sikorski.

View Article and Find Full Text PDF

Research on the very specific damage to single textile fibres caused by vapour cloud explosions is presented. Vapour cloud explosion experiments were carried out using a selection of 41 garments differing in colour, fibre composition and textile construction. Fibres subjected to a vapour cloud explosion become wider at the end, often taking the form of a ball, bulb or shovel, while the morphological structure of the remaining part of the fibre remains almost unchanged.

View Article and Find Full Text PDF