An automated instrument for improving the sensitivity of nuclear quadrupole resonance (NQR) spectroscopy is presented. The device is capable of pre-polarizing samples within a custom Halbach-type permanent magnet and then moving them into an external probe for zero-field NQR detection. Polarization transfer between protons and nitrogen (N) nuclei in the sample occurs during demagnetization, thus increasing the amplitude of the detected NQR signals.
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