This study presents a novel approach for the rapid and reliable electrochemical determination of 5-hydroxymethylfurfural (5-HMF) in honey using a screen-printed carbon electrode modified with nickel oxide nanoparticles (NiONPs/SPCE). The NiONPs were synthesized using a simple method and characterized using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The NiONPs/SPCE demonstrated enhanced sensitivity and selectivity for 5-HMF detection.
View Article and Find Full Text PDFA portable paper-based electrochemical sensor has been developed to determine 5-hydroxymethylfurfural (5-HMF). A screen-printed carbon electrode (SPCE) was facilely fabricated for the first time on poster paper which showed a very satisfactory electrochemical response. The analytical performance of the electrode was enhanced by electrochemical deposition of silver microdendrites (AgMDs).
View Article and Find Full Text PDFA label-free electrochemical aptamer-based sensor has been fabricated for alpha-fetoprotein (AFP) detection. Platinum nanoparticles on carboxylated-graphene oxide (PtNPs/GO-COOH) modified screen-printed graphene-carbon paste electrode (SPGE) was utilized as an immobilization platform, and the AFP aptamer was employed as a bio-recognition element. The synthesized GO-COOH helps to increase the surface area and amounts of the immobilized aptamer.
View Article and Find Full Text PDFA simple, rapid, and cost-effective flow injection amperometric (FI-Amp) sensor for sensitive determination of uric acid (UA) was developed based on a new combination of carbon black (CB) and graphene oxide (GO) modified screen-printed carbon electrode (SPCE). The CB-GO nanocomposites were simply synthesized and modified on the working electrode surface to increase electrode conductivity and enhance the sensitivity of UA determination via the electrocatalytic activity toward UA oxidation. The morphologies and electrochemical properties of the synthesized nanomaterials were investigated through scanning electron microscopy (SEM), transmission electron microscopy (TEM), electrochemical impedance spectroscopy (EIS), and cyclic voltammetry (CV).
View Article and Find Full Text PDFIn this research work, a non-enzymatic amperometric sensor for the determination of glucose was designed based on carbon nanodots (C-dots) and copper oxide (CuO) nanocomposites (CuO-C-dots). The CuO-C-dots nanocomposites were modified on the surface of a screen-printed carbon electrode (SPCE) to increase the sensitivity and selectivity of the glucose sensor. The as-synthesized materials were further analyzed for physico-chemical properties through characterization tools such as transmission electron microscopy (TEM) and Fourier-transform infrared spectroscopy (FTIR); and their electrochemical performance was also studied.
View Article and Find Full Text PDFFlow injection amperometric (FI-Amp) sensor was developed for sensitive and selective determination of hydroquinone. A simple screen printed carbon electrode (SPCE) was modified with various nanomaterials for improvement of sensitivity on the determination of quinone. As a result, the appropriate sensitivity is obtained from the SPCE modified with carbon nanotube (CNT) which indicated that CNT contributed to the transfer of electron to quinone.
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