Herein, we report the fabrication of zinc oxide nanowire (ZnO NW) coated carbon fiber (CF) ultra-microelectrodes (UME). ZnO NWs were grown on commercial multifilament CFs through hydrothermal process in a teflon-lined autoclave at 90 °C for 4 h. X-ray diffraction (XRD), Raman and scanning electron microscopy characterizations showed that crystalline and well oriented NW structures were successfully obtained.
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