Microsc Res Tech
November 2024
Analysis of indentation data of heterogeneous material, in particular, layer on an elastic substrate requires information about the contact area that is essential for calculating mechanical properties. The actual shape of the AFM-tip is not described by simple body of revolution. In this work, the indentation of a stiff layer on a hyperelastic substrate by a truncated conical tip is studied using finite element methods.
View Article and Find Full Text PDFPolymer materials are widely used in medicine due to their mechanical properties and biological inertness. When ion-plasma treatment is used on a polymer material, a carbonization process occurs in the surface nanolayer of the polymer sample. As a result, a surface carbonized nanolayer is formed, which has mechanical properties different from those of the substrate.
View Article and Find Full Text PDFMicrosc Res Tech
January 2024
Reliable reconstruction of AFM tip geometry is not an easy task. The shape of the tip can be (partially) reconstructed from the AFM image of a calibration sample using a blind reconstruction method. The result is a range of the tip shapes (from unrealistically sharp to blunt).
View Article and Find Full Text PDFNanocoatings formed by various plasma and chemical methods on the surface of polymeric materials have unique properties. However, the applicability of polymeric materials with nanocoatings under specific temperature and mechanical conditions depends on the physical and mechanical properties of the coating. The determination of Young's modulus is a task of paramount importance since it is widely used in calculations of the stress-strain state of structural elements and structures in general.
View Article and Find Full Text PDFWe have investigated the evolution of the structure and surface morphology of n-ZnO/p-ZnO homojunctions and n-ZnO/p-NiO heterojunctions transparent structures deposited by radio frequency-sputtering on quartz (Q)/ITO substrates. X-ray diffraction (XRD) analysis of the as-deposited and annealed ZnO, n-ZnO/p-NiO/Q/ITO, and n-ZnO/p-ZnO/Q/ITO thin films showed that ZnO had a wurtzite hexagonal structure and (002) preferred growth direction. The annealing temperature played a key role in improving the crystalline structure of the films, as evidenced by the changes in the intensity and position of the XRD (002) peak.
View Article and Find Full Text PDFMicrosc Res Tech
September 2021
Modern techniques of nanoindentation by atomic force microscopy (AFM) produce maps of topography and physical-mechanical properties of the material. Analysis of the interaction rate of the AFM tip with the soft surface reveals the surface and subsurface structure and expands standard analysis of the material behavior. Phase-separated polymer (polyurethane, elastic modulus-6 MPa) is studied.
View Article and Find Full Text PDFThe main goal of the present work is to explore the three dimensional (3-D) atomic force microscopy (AFM) images of human teeth and investigating their micromorphology. For this purpose, 10 fresh and permanent canine teeth were selected from a group of 40-year-old men who were candidate for the experimental processes. Afterward, they were all applied for studying the morphology of their hard tissues.
View Article and Find Full Text PDFThe objective of this study is the experimental investigation of the silver in diamond-like carbon (Ag/DLC) nanocomposite prepared by the co-deposition of radio frequency plasma-enhanced chemical vapor deposition (RF-PECVD) and RF-sputtering. Atomic force microscopy (AFM), X-ray diffraction analyses, ultraviolet-visible (UV-visible) spectroscopy measurements were applied to describe the three-dimensional surface texture data in connection with the statistical, and multifractal analyses. Additional information about structure-property relationships in prepared Ag/DLC nanocomposite was studied in detail to allow a better understanding of the surface micromorphology.
View Article and Find Full Text PDFA lot of insect families have physical structures created by evolution for coloration. These structures are a source of ideas for new bio-inspired materials. The aim of this study was to quantitatively characterize the micromorphology of butterfly wings scales using atomic force microscopy and multifractal analysis.
View Article and Find Full Text PDFThe surface of elastic polyurethane treated by plasma immersion N2(+) ion implantation at different fluences has been investigated. A folded surface structure is observed in all cases. Analysis has been performed to study the structural (roughness, steepness and fraction of folds, fractal characteristics), mechanical (stiffness, adhesion force between the AFM probe and the material) and wetting properties of surfaces.
View Article and Find Full Text PDFThe influence of soluble and immobilized plasma, albumin, and fibronectin (Fn) on the adhesion of three Staphylococcus epidermidis strains to polystyrene was investigated. Both soluble and immobilized plasma and albumin cause to 7-fold reduction of the amounts of adhered cells, regardless of the strain used. The soluble Fn exhibited the adhesion for one strain and did not affect the bacterial sorption for remaining strains, whereas on Fn-coated polystyrene two of the three strains showed about 1.
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