Bond strength of 4META-MMA-TBB resin to a CAD/CAM composite resin block and analysis of acetone-insoluble cured resin residues at adhesive interfaces.

This study investigated the adhesion of 4META-MMA-TBB resin to CAD/CAM composite resin blocks. CAD/CAM composite resin blocks were subjected to alumina blasting, ceramic primer treatment, or both, and then bonded with 4META-MMA-TBB resin. The tensile bond strength of 4META-MMA-TBB resin to blocks without surface treatment was approximately 20 MPa, but with surface treatment, it significantly improved to approximately 40 MPa.

Evaluation of the effects of three pretreatment conditioners and a surface preparation system on the bonding durability of composite resin adhesive to a gold alloy.

This study aimed to evaluate the effect of three pretreatment conditioners and surface preparations on a composite resin adhesive for a gold alloy. Cast disk specimens were made and bonded with RelyX Unicem luting agent under six surface conditions: 1) polished with No.600 carbide paper, 2) air-abraded with alumina, 3) Alloy Primer metal conditioner was applied after alumina-abrasion, 4) Monobond Plus multipurpose conditioner was applied after alumina-abrasion, 5) M.

Bonding durability between acrylic resin adhesives and titanium with surface preparations.

The purpose of the present study was to evaluate the efficacy of pretreatment on the bonding durability between titanium casting and two acrylic adhesives. Cast titanium disk specimens treated with four polymer-metal bonding systems as follow: 1) air-abraded with 50-70 μm alumina, 2) 1)+Alloy Primer, 3) 1)+M.L.

Effects of polymerization method on flexural and shear bond strengths of a fiber-reinforced composite resin.

This study investigated the effects of indirect composite polymerization on the postcuring mechanical properties of a fiber-reinforced composite. An indirect composite seated on glass fibers preimpregnated with polymerized monomer was polymerized by 1) photoirradiation using a halogen-fluorescent polymerizing unit for 5 min, 2) method 1 plus secondary heating at 100°C for 15 min, 3) photoirradiation using a metal halide light unit for 60 s, or 4) preliminary polymerization using a halogen light unit for 20 s followed by method 3. After polymerization, the flexural and shear bond strengths of the fiber-reinforced composite were examined, as was the flexural strength of non-fiber-reinforced composite specimens polymerized using the same methods.

Factors affecting the bond strength of denture base and reline acrylic resins to base metal materials.

Objective: The shear bond strengths of two hard chairside reline resin materials and an auto-polymerizing denture base resin material to cast Ti and a Co-Cr alloy treated using four conditioning methods were investigated.

Material And Methods: Disk specimens (diameter 10 mm and thickness 2.5 mm) were cast from pure Ti and Co-Cr alloy.

Evaluation of a newly developed polymethyl methacrylate powder for brush-dip technique.

Purpose: The aim of this study is to evaluate a newly developed polymethyl methacrylate (PMMA) powder.

Methods: The particle size distribution, surface area, and particle shape of both new and traditional powders were compared. The shear bond strength of the resin cement with the new powder to a silver-palladium-copper-gold alloy was determined and compared to that for a cement with the traditional powder.

Bond strength of poly(methyl methacrylate) denture base material to cast titanium and cobalt-chromium alloy.

Purpose: The shear bond strength of an auto-polymerizing poly(methyl methacrylate) denture base resin material to cast titanium and cobalt-chromium alloy treated with six conditioning methods was investigated.

Materials And Methods: Disk specimens (10 mm in diameter and 2.5 mm in thickness) were cast from pure titanium and cobalt-chromium alloy.

Evaluation of two dual-functional primers and a tribochemical surface modification system applied to the bonding of an indirect composite resin to metals.

We evaluated the effects of two dual-functional primers and a tribochemical surface modification system on the bond strength between an indirect composite resin and gold alloy or titanium. Disk specimens (diameter, 10 mm; thickness, 2.5 mm) were cast from type 4 gold alloy and commercially pure titanium.

Influence of centrifugal force on filler loading of resin composites.

This study examined the influence of centrifugal force on the filler loading of composites using a light-polymerizing apparatus combined with a centrifuge. To assess uneven filler particle distribution resulting from specimen rotation, two low-viscosity composites (Palfique Estelite LV and Revolution Formula 2) were placed in test tubes, centrifuged, and subsequently light-polymerized with the apparatus. After each specimen was sliced into four disks (2-mm thickness), the inorganic filler content and Knoop hardness number (KHN) of each disk were determined.

Bond strength to primed Ti-6Al-7Nb alloy of two acrylic resin adhesives.

This study aimed to evaluate the bonding behavior of two acrylic resin adhesives joined to titanium-aluminum-niobium (Ti-6Al-7Nb) alloy primed with two metal conditioners. Cast Ti-6Al-7Nb alloy disks were air-abraded with alumina and bonded with six combinations of two resin adhesives (Super-Bond C&B and Multi Bond) and three surface conditions (Alloy Primer, M.L.

Evaluation of 2 thione primers and 3 resin adhesives for silver-palladium-copper-gold alloy bonding.

Objective: The purpose of this study was to evaluate 2 thione primers and 3 resin adhesives for enhancement of bonding strength to a silver-palladium-copper-gold alloy.

Method And Materials: Two different sized disk specimens (10- and 8-mm diameter by 2.5-mm thick) were prepared from a silver-palladium-copper-gold alloy (Castwell M.

Twenty-four hour bond strength between layers of a highly loaded indirect composite.

This study evaluated the repair bond strength of Estenia composite. Disk specimens of a dentin material were conditioned with varying combinations of silane primer (Add-on Primer, Clearfil Porcelain Bond Activator, Clearfil Porcelain Bond Activator + Clearfil Mega Bond-Primer, Porcelain Liner M, and unprimed) and bonding agent (Clearfil Mega Bond-Bond, Modeling Liquid, Stain Diluent, and no bonding agent). After photopolymerization of the enamel material placed on each surface, the specimens were either wet- or dry-stored at 37 degrees C for 24 hours.

Effectiveness of bonding systems on bonding durability of a prefabricated porcelain material.

The purpose of the present study was to evaluate the bond strength and durability of four bonding systems joined to a prefabricated porcelain material (Vita Celay Blanks). Two sizes of porcelain block were bonded with one of the following systems: (1) Clapearl Bonding Agent and Clapearl DC; (2) Imperva Porcelain Primer and Imperva Dual; (3) Monobond S and Variolink II; or (4) Tokuso Ceramics Primer and Bistite II. Shear bond strength was measured after 24-hour immersion in water and after subsequent thermocycling.

Color stability of acrylic resin adhesives with different initiation modes.

The purpose of this study was to evaluate the color stability of two acrylic resin adhesives with different activation systems: a benzoyl peroxide (BPO)-amine redox system and a tri-n-butylborane (TBB) derivative system. The colorimetric values of the two resins in different shades (Clear and Ivory) were determined (n=5) 24 hours after polymerization as a baseline using the L*a*b* system of the Commission Internationale de l'Eclairage (CIE). The specimens were thereafter immersed in distilled water, and the color difference (deltaE*) values were calculated.

Effects of a fluoride etchant on resin bonding to titanium-aluminum-niobium alloy.

This investigation was carried out in order to evaluate ammonium hydrogen fluoride (AHF) and cupric chloride (CC) as components of a metal etchant. The surface of cast titanium-aluminum-niobium (Ti-6Al-7Nb) was air-abraded with alumina, etched for 10 s, and rinsed with water. A phosphate or a thiophosphate primer was applied to the bonding area, and an acrylic rod was bonded to the specimen with a tri-n-butylborane-initiated self-curing luting agent.

Effects of a metal etchant and two primers on resin bonding durability to titanium.

The purpose of this study was to investigate the efficacy of an etchant in titanium bonding. The aqueous etchant consisted of 0, 5, or 10 wt% ammonium hydrogen fluoride (AHF) in combination with 0, 0.03, 0.

Adhesive bonding of titanium-aluminum-niobium alloy with nine surface preparations and three self-curing resins.

The purpose of the current study was to evaluate the adhesive performance of metal conditioners when used for bonding between auto-polymerizing methacrylic resins and a titanium alloy. Disk specimens were cast from a titanium-aluminum-niobium (Ti-6Al-7Nb) alloy, air-abraded with alumina, and bonded with 24 combinations of eight metal conditioners (Acryl Bond, ACB; All-Bond 2 Primer B, ABB; Alloy Primer, ALP; Cesead II Opaque Primer, COP; Metafast Bonding Liner, MBL; Metal Primer II, MPII; MR Bond, MRB; Super-Bond liquid, SBL) and three autopolymerizing methacrylic resins (Repairsin, RE; Super-Bond C & B, SB; Tokuso Rebase; TR). Unprimed specimens were used as controls.