Electropolymerization of 3,4-(2-benzylpropylene)-dioxythiophene (ProDOT-Bz) on (approximately 7 microm diameter) single carbon fiber microelectrodes (SCFMEs) in different electrolytes resulted the network of nanofiber structure. Electropolymerization performed in different electrolytes by using cyclovoltammetric technique. Surface morphology of coatings was investigated by Scanning Electron Microscopy (SEM), the attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) was used for the characterization.
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