The present study aimed to analyze simultaneous biosorption of Cd and Ni by living Phanerochaete chrysosporium as low-cost and eco-friendly biosorbent following optimization by applying a central composite design. The effect of operating parameters such as solution pH (4.0-8.
View Article and Find Full Text PDFIn this research, a facile synthesis route was used for preparation of cobalt ferrite@SiO@polyethyleneimine magnetic nanoparticles (Co-FeO@PEI) as a new sorbent in the service of ultrasound assisted dispersive micro-solid phase extraction (UA-DMSPME) for influential clean-up, preconcentration, and determination of tartrazine (TA) prior to UV-Vis spectrophotometric detection. The understudy sorbent was fully characterized by transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), Energy dispersive X-ray analysis (EDX), and vibrating sample magnetometer (VSM). Different operating parameters which affected the extraction efficiency of TA viz.
View Article and Find Full Text PDFJ AOAC Int
April 2013
The efficiency of modified activated carbon (AC) and multiwalled carbon nanotubes (MWCNTs) for the separation/preconcentration and determination of Co, Cd, Pb, Zn, and Cu following their complexation by bis(3-nitrobenzylidene)-1,2-ethanediamine has been described and compared. A one-at-a-time optimization method investigated the influence of various parameters that significantly influence the recoveries of the studied metal ions. At the optimum values of all variables, the response was linear over the range of 0.
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