Early detection of significant abnormal changes is highly desirable for oil refinery processes, which consist of sophisticated unit operations handling hazardous and flammable inventories and operating at high temperature and pressure. Close monitoring and anomaly detection are vital for avoiding major accidents and losses and enable intervention before failure occurrence. A new big data analytics tool called Plant Health Index (PHI) is proposed in this work.
View Article and Find Full Text PDFThermogravimetric analysis (TGA) was employed to investigate the thermal stability of asphaltenes at different environments (inert and oxidizing atmosphere) and identify their refractory nature. TGA and differential scanning calorimetry were carried out at a temperature range of 50-700 °C, for asphaltene samples obtained from atmospheric residues, vacuum residues (VRs), and aromatic petroleum pitch samples, which were obtained from the cracking of VRs at different temperatures. The TGA results clearly indicate that thermal degradation of asphaltene takes place in a single process that starts around 350 °C and ends at 500 °C, giving ash contents of less than 2%.
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