Real-time monitoring of the structural evolution of battery materials is crucial for understanding their underlying reaction mechanisms, which cannot be satisfied by the typically used post-mortem analysis. While more and more techniques were constructed and employed, they are all based on ambient working conditions that are not generally the case for real-world applications. Indeed, batteries work in an environment where self-heat dissipation increases the surrounding temperature, and extreme temperature applications (<-20 °C or >60 °C) are also frequently proposed.
View Article and Find Full Text PDFIn this work, a total of 18 types of choline chloride, betaine, and L-proline-based deep eutectic solvents (DESs) were synthesized to determine the extraction yield of a natural polysaccharide (PSA) from Dysosma versipellis using an ultrasound-assisted extraction method. Results indicate that the choline-oxalic acid-based DES has the best extraction yield for PSA due to the proper physical-chemical properties between PSA and DES. To evaluate the optimal extraction conditions, a response surface methodology was carried out.
View Article and Find Full Text PDFJ Nanosci Nanotechnol
December 2019
A novel Eu-TiO₂ nanocomposite prepared by a sol-gel method is used for the degradation of rhodamine B (RhB) present in dyes wastewater. The X-ray diffraction (XRD), Raman spectroscopy and transmission electron microscopy (TEM) show the anatase phase and globular shape of Eu- TiO₂ nanocomposite, UV-vis diffuse reflectance spectroscopy and low temperature N₂ adsorption (BET) indicate Eu-TiO₂ possesses a narrow band gap (2.98 eV) and a high specific surface area (112.
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