Publications by authors named "Gulchekhra Shakirova"

A probing study to establish a reliable and robust method for determining the iodine concentration using the ELAN DRC II ICP-MS was performed in combination with a sample digestion and filtration step. Dairy products from locally available sources were evaluated to help determine the possibility and need for further evaluations in relation to the U.S.

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During the Ebola virus outbreak of 2013-2016, the Viral Special Pathogens Branch field laboratory in Sierra Leone tested approximately 26 000 specimens between August 2014 and October 2015. Analysis of the B2M endogenous control Ct values showed its utility in monitoring specimen quality, comparing results with different specimen types, and interpretation of results. For live patients, blood is the most sensitive specimen type and oral swabs have little diagnostic utility.

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Article Synopsis
  • A new radiochemical neutron activation analysis (RNAA) method was developed to measure arsenic levels in standard reference materials (SRMs) for blood and urine samples.
  • Samples were freeze-dried, irradiated, and analyzed using gamma-ray spectroscopy after separating arsenic from other materials.
  • The results were standardized with values from other labs, yielding certified arsenic concentrations for several levels in the SRMs, while an information value was assigned for one level due to measurement discrepancies.
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Biomonitoring and emergency response measurements are an important aspect of the Division of Laboratory Sciences of the National Center for Environmental Health, Centers for Disease Control and Prevention (CDC). The continuing advancement in instrumentation allows for enhancements to existing analytical methods. Prior to this work, chromium and nickel were analyzed on a sector field inductively coupled plasma-mass spectrometer (SF-ICP-MS).

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