Characterization and preparation of p(U-MMA-An) interpenetrating polymer network damping and absorbing material.

P(U-MMA-ANI) interpenetrating polymer network (IPN) damping and absorbing material is successfully synthesized by PANI particles served as an absorbing agent with the microemulsion polymerization and P(U-MMA) foam IPN network structure for substrate materials with foaming way. P(U-MMA-ANI) IPN is characterized by the compression mechanical performance testing, TG-DSC, and DSC. The results verify that the P(U-MMA) IPN foam damping material has a good compressive strength and compaction cycle property, and the optimum content of PMMA was 40% (mass) with which the SEM graphs do not present the phase separation on the macro level between PMMA and PU, while the phase separation was observed on the micro level.

Preparation and characterization of novel anion phase change heat storage materials.

In this paper, polyurethane phase change material was successfully prepared with TDI with BDO for hard segments and PEG for soft segments. Moreover, based on this the solid-solid phase change material, A-PCM1030 which can release anions was prepared with the successful addition of anion additives A1030 for the first time. Then the test of the above material was conducted utilizing FT-IR, DSC, TEM, WAXD and Air Ion Detector.

Preliminary study on the preparation of bamboo cellulose carbamate.

In this paper, bamboo fibers were utilized in synthesizing the cellulose carbamate (CC) together with urea for the first time. This paper explored the impact of a serious of factors on Nitrogen content of CC, including the concentration of sodium hydroxide solution used for activating, activation time, aging time, urea socking time, the concentration of urea solution, reaction time and reaction temperatures. Moreover, the analysis and characterizations of CC with different nitrogen contents were conducted by using FTIR, DSC, XRD and SEM.

[FTIR spectra study on the film of polyurethane coated urea controlled-release fertilizer].

The polyurethane films were prepared to wrap the urea in order to achieve a desirable release rate by mixing isocyanate, polyols and wax. The effect of wax, urea and isocyanate on the structure and properties of the films was investigated by FTIR. The structural changes were monitored as the polyurethane films together with the wrapped urea were immersed into ammonia water for 28 days, which is used to model soil conditions.

2',10'-Dibromo-spiro-[cylohexane-1,6-di-benzo[d,f][1,3]dioxepine].

In the title compound, C(18)H(16)Br(2)O(2), the dihedral angle between the aromatic rings is 35.55 (17)° and the cyclohexyl ring adopts a chair-like conformation. In the crystal, molecules are linked by van der Waals forces.