Formation of crystalline Na2V6O16·3H2O ribbons into belts and rings.

Single-crystalline nanobelts and nanorings of Na(2)V(6)O(16)·3H(2)O structures have been facilely synthesized through a direct hydrothermal reaction between NaVO(3) and H(3)PO(4), without the addition of any harmful solvents or surfactants. The analytical techniques of scanning electron microscopy, transmission electron microscopy (TEM), powder X-ray diffraction, thermogravimetric analysis, energy-dispersive X-ray spectroscopy, Fourier transform infrared, high-resolution TEM, and selected-area electron diffraction have been used to characterize the morphology, composition, and structure of the synthesized products. The Na(2)V(6)O(16)·3H(2)O nanobelts are up to several hundreds of micrometers in length and 100-300 nm in thickness, and for nanorings, the diameters are 4.

Morphological evolution of (NH4)(0.5)V2O5·mH2O fibers into belts, triangles, and rings.

In this contribution, single-crystalline (NH(4))(0.5)V(2)O(5)·mH(2)O xerogels made of belts, rings, triangles, and ovals have been synthesized using a surfactant-free hydrothermal method. The analytical techniques of scanning electron microscopy (SEM), transmission electron microscopy (TEM), powder X-ray diffraction (PXRD), thermogravimetric analysis (TGA), energy dispersive X-ray spectroscopy (EDX), Fourier transform infrared (FTIR), high-resolution TEM (HRTEM), and selected area electron diffraction (SAED) have been used to characterize the morphology, composition, and structure of the as-prepared products.

Heavy metals content in water, water hyacinth and sediments of Lalbagh tank, Bangalore (India).

The present study was undertaken for assessing the level of heavy metals such as iron, zinc, copper, nickel, chromium, lead and cadmium in water, water hyacinth and sediment samples of Lalbagh tank, Bangalore. Metals were detected using flame atomic absorption spectrophotometry. The results revealed that by and large all metals are present in all the samples, except cadmium in the sediment samples.

Nanocrystalline CaO as adsorbent to remove COD from paper mill effluent.

Porous nanocrystalline CaO has been prepared by the solution combustion process using calcium nitrate as oxidizer and glycine as a fuel. As prepared calcium oxide has been characterized using powder X-Ray Diffraction (XRD), BET surface area, and Scanning Electron Microscopy (SEM). The powder XRD pattern confirms the crystallinity and phase purity of the powder.

Hydrothermal synthesis of amorphous MoS2nanofiber bundles via acidification of ammonium heptamolybdate tetrahydrate.

MoS2nanofiber bundles have been prepared by hydrothermal method using ammonium molybdate with sulfur source in acidic medium and maintained at 180 °C for several hours. The obtained black crystalline products are characterized by powder X-ray diffraction (PXRD), Fourier transform infrared spectrometer (FTIR), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The PXRD pattern of the sample can be readily indexed as hexagonal 2H-MoS2.