The paper presents a novel instrumental analytical endotoxin quantification assay. It uses common analytical laboratory equipment (HPLC-FLD) and allows quantifying endotoxins (ETs) in different matrices from about 109 EU per mL down to about 40 EU per mL (RSE based). Test results are obtained in concentration units (e.
View Article and Find Full Text PDFMultiferroic composite materials combining ferroelectric and ferromagnetic order at room temperature have great potential for emerging applications such as four-state memories, magnetoelectric sensors, and microwave devices. In this paper, we report an effective and facile liquid phase deposition route to create multiferroic composite thin films involving the spin-coating of nanoparticle dispersions of BaTiO, a well-known ferroelectric, and CoFeO, a highly magnetostrictive material. This approach offers great flexibility in terms of accessible film configurations (co-dispersed as well as layered films), thicknesses (from 100 nm to several μm) and composition (5-50 wt % CoFeO with respect to BaTiO) to address various potential applications.
View Article and Find Full Text PDFTexturing of magnetic ceramics and composites by aligning and fixing of colloidal particles in a magnetic field is a powerful strategy to induce anisotropic chemical, physical and especially mechanical properties into bulk materials. If porosity could be introduced, anisotropically structured magnetic materials would be the perfect supports for magnetic separations in biotechnology or for magnetic field-assisted chemical reactions. Aerogels, combining high porosity with nanoscale structural features, offer an exceptionally large surface area, but they are difficult to magnetically texture.
View Article and Find Full Text PDFAerogels with their low density and high surface area are fascinating materials. However, their advantageous morphology is still far from being fully exploited owing to their limited compositional variety and low crystallinity. Replacing the sol-gel process by a particle-based assembly route is a powerful alternative to expand the accessible functionalities of aerogels.
View Article and Find Full Text PDFNonaqueous synthesis routes have emerged as a powerful platform for directly obtaining diverse metal oxide nanoparticles with high crystallinity and tunable compositions. The benzyl alcohol (BA) route, for example, has been applied toward dozens of oxides including binary, ternary, and even more complex multimetal systems. Here we compare anatase nanoparticles made from the BA route with the traditional hydrothermal route.
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