Multi-elemental analysis of commercial wheat flours by ICP-MS triple quadrupole in function of the milling degree.

This preliminary study is focused on an elemental analysis of 60 samples of different commercial grains' flour, including various typologies of refined product, researching transition metals and trace elements. All the samples were first digested with a microwave digestion system and then analyzed by a triple quadrupole (TQ) inductively coupled plasma mass spectrometer (ICP-MS-QQQ) located in a Clean Room ISO class 6. The minimum value of most of the elements (Li, Be, Na, Ca, V, Cr, Mn, Fe, Co, Ni, Zn, Ga, As, Se, Rb, Sr) are in the wheat flour "00" type and in the wheat flour "0" type (B, Na, Mg, Al, Cu, Ag, Cd, In, Cs, Pb, Bi).

Preparation and Characterization of Isostructural NaMoO and NaWO and a Study of the Composition of Their Mixed System.

NaMoO and NaWO are isostructural semiconductors, belonging to the spinel class. They have interesting properties and find applications in numerous sectors. These properties can be tuned by controlling the composition of their solid solutions.

Halide Perovskites Films for Ionizing Radiation Detection: An Overview of Novel Solid-State Devices.

Halide perovskites are a novel class of semiconductors that have attracted great interest in recent decades due to their peculiar properties of interest for optoelectronics. In fact, their use ranges from the field of sensors and light emitters to ionizing radiation detectors. Since 2015, ionizing radiation detectors exploiting perovskite films as active media have been developed.

Dissolution of Molybdenum in Hydrogen Peroxide: A Thermodynamic, Kinetic and Microscopic Study of a Green Process for Tc Production.

Tc-based radiopharmaceuticals are the most commonly used medical radioactive tracers in nuclear medicine for diagnostic imaging. Due to the expected global shortage of Mo, the parent radionuclide from which Tc is produced, new production methods should be developed. The SORGENTINA-RF (SRF) project aims at developing a prototypical medium-intensity D-T 14-MeV fusion neutron source specifically designed for production of medical radioisotopes with a focus on Mo.

Set up and test of an anticoincidence system for the detection of radioactive xenon by gamma spectrometry system.

The aim of this work is based on the optimisation of a gamma spectrometry system in anticoincidence for the detection of noble gases, in particular the radioactive isotopes of xenon. These four radionuclides are of particular interest for the Comprehensive Nuclear Test-Ban Treaty (CTBT). The Laboratory of the ENEA Research Centre of Brasimone, where the experimental apparatus has been set up to carry out the measurements of Xe, Xe, Xe and Xe, is able to provide, if necessary, data and analysis on noble gases.

Forensic Analysis of Commercial Inks by Laser-Induced Breakdown Spectroscopy (LIBS).

Laser-induced breakdown spectroscopy (LIBS) was tested for all of the relevant issues in forensic examinations of commercial inks, including classification of pen inks on one paper type and on different paper types, determination of the deposition order of layered inks, and analysis of signatures and toners on one questioned document. The scope of this work was to determine the potential of a single LIBS setup that is compatible with portable instruments for different types of ink analysis, rather than building a very large database for inks and papers. We identified up to seven metals characteristic for the examined inks, which allowed to fully discriminate all eight black inks on one type of printing paper.