The aim of this study was to evaluate the influence of boron-nitride nanotubes (BNNTs) on the properties of resin-based light-curing dental sealants (RBSs) when incorporated at different concentration. RBSs were formulated using methacrylate monomers (90 wt.% TEGDMA, 10 wt.
View Article and Find Full Text PDFThis in situ study aimed to evaluate the antibacterial and anti-demineralization effects of an experimental orthodontic adhesive containing triazine and niobium phosphate bioglass (TAT) around brackets bonded to enamel surfaces. Sixteen volunteers were selected to use intra-oral devices with six metallic brackets bonded to enamel blocks. The experimental orthodontic adhesives were composed by 75% BisGMA and 25% TEGDMA containing 0% TAT and 20% TAT.
View Article and Find Full Text PDFOrthodontic adhesives with antimicrobial and remineralizing properties may be an alternative to control white spot lesions around brackets. The aim of this study is to develop an experimental orthodontic adhesive containing boron nitride nanotubes (BNNT) and alkyl trimethyl ammonium bromide (ATAB). Methacrylate (BisGMA and TEGDMA) monomers were used to formulate the adhesives.
View Article and Find Full Text PDFThe aim of this study was to evaluate enamel roughness, quality of the enamel surfaces and time duration comparing different orthodontic adhesive removal protocols. Premolars were used to test three adhesive removal methods ( = 20): five-blade carbide bur, 30-blade carbide bur, and ultrasonic diamond bur. Bracket was bonded using Transbond XT adhesive.
View Article and Find Full Text PDFThis study is aimed at evaluating the effects of triclosan-encapsulated halloysite nanotubes (HNT/TCN) on the physicochemical and microbiological properties of an experimental dental composite. A resin composite doped with HNT/TCN (8% /), a control resin composite without nanotubes (HNT/TCN-0%) and a commercial nanofilled resin (CN) were assessed for degree of conversion (DC), flexural strength (FS), flexural modulus (FM), polymerization stress (PS), dynamic thermomechanical (DMA) and thermogravimetric analysis (TGA). The antibacterial properties (M) were also evaluated using a 5-day biofilm assay (CFU/mL).
View Article and Find Full Text PDFObjective: The aim of this study was to evaluate physicochemical properties, long-term microtensile bond strength and cytotoxicity of methacrylate-based adhesive containing boron nitride nanotubes (BNNTs) as fillers.
Methods: A dental adhesive was formulated using BisGMA/HEMA, 66/33wt% (control). Inorganic BNNT fillers were incorporated into the adhesive at different concentrations (0.
Objective: To evaluate the immediate enamel bond strength, in situ degree of conversion and the polymerisation rate of three experimental orthodontic adhesives containing triclosan-loaded halloysite nanotubes. The antibacterial and bioactivity properties of such experimental materials were also assessed.
Materials And Methods: Three experimental orthodontic adhesives were formulated by incorporating triclosan-loaded halloysite nanotubes (TCN-HNT) at different concentrations (5wt%, 10wt% and 20wt%) into a resin blend (Control).
Objective: This study aimed to evaluate the physical-chemical properties of experimental dental adhesives containing boron nitride nanotubes (BNNTs) as inorganic fillers.
Methods: An experimental adhesive resin was prepared using HEMA-BisGMA, 66/33wt% (control). Inorganic BNNT fillers were first analyzed using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) and then incorporated into the adhesive at different concentration (0.
Objective: This study aimed to incorporate silver nanoparticle solutions (AgNP) in an orthodontic adhesive and evaluate its physicochemical and antimicrobial properties.
Material And Methods: Silver nanoparticle solutions were added to a commercial adhesive in different concentrations (w/w): 0%, 0.11%, 0.
Objective: This study aimed to assess the degree of conversion, microhardness, solvent degradation, contact angle, surface free energy and bioactivity (e.g., mineral precipitation) of experimental resin-based materials containing, pure or triclosan-encapsulated, aluminosilicate-(halloysite) nanotubes.
View Article and Find Full Text PDFObjective: To determine the consensus among studies that adhesive resin application improves the bond strength of orthodontic brackets and the association of methodological variables on the influence of bond strength outcome.
Materials And Methods: In vitro studies were selected to answer whether adhesive resin application increases the immediate shear bond strength of metal orthodontic brackets bonded with a photo-cured orthodontic adhesive. Studies included were those comparing a group having adhesive resin to a group without adhesive resin with the primary outcome measurement shear bond strength in MPa.
This in vitro study sought to evaluate how surface conditioning from bracket and mechanical cycling aging affected the bond strength between metallic brackets and bovine enamel, and to determine the adhesive remnant index. Eighty bovine incisors were embedded in acrylic resin using polyvinyl chloride rings and divided into 4 groups based on surface treatment (n = 20). Group 1 (control) received no surface treatment, Group 2 specimens were sandblasted with aluminum oxide particles, Group 3 specimens were sandblasted with silicon oxide and treated with a tribochemichemical silica coupling agent, and Group 4 specimens were primed with a multidomain protein-based agent.
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