Crystallization and particle size distribution of hydrothermally synthesized SAPO-34: an experimental and population balance study.

A population balance-based model was developed to describe the crystallization kinetics of the SAPO-34 zeotype through the hydrothermal method at three distinct temperatures of 180, 200, and 220 °C. The synthesized SAPO-34 catalysts were characterized by XRD, FESEM, BET, and DLS analysis. The model was constructed based on XRD patterns and incorporated established kinetic expressions for homogeneous nucleation and diffusion-controlled crystal growth.

An investigation of the crystallization kinetics of zeotype SAPO-34 crystals synthesized by hydrothermal and sonochemical methods.

The kinetics study of SAPO-34 crystallization from a gel containing morpholine as a structure directing agent (SDA) was investigated by means of X-ray diffraction (XRD) patterns in order to determine the kinetics parameters, i.e. induction times, rate constants, frequency factors, and activation energies for the induction and growth stages.