Publications by authors named "F Niculescu"

The experimental research was focused on the investigation of valuable material from spent Ni-MH type AA batteries, namely the metal grid anodes and the black mass material (anode and cathode powder). The materials of interest were analyzed by X-ray fluorescence spectroscopy (XRF), ICP-OES (inductively coupled plasma optical emission spectrometry), optical microscopy, scanning electron microscopy (SEM), energy-dispersive X-ray analysis (EDX), electron backscatter diffraction (EBSD), and X-ray diffraction (XRD). The analyzed grids have a high Fe content, but some of them correspond to the Invar alloy with approx.

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Properties such as lower melting temperature, good tensile strength, good reliability, and well creep resistance, together with low production cost, make the system Bi-Sn an ideal candidate for fine soldering in applications such as reballing or reflow. The first objective of the work was to determine the thermodynamic quantities of Bi and Sn using the electromotive force measurement method in an electrolytic cell (Gibbs' enthalpies of the mixture, integral molar entropies, and the integral molar excess entropies were determined) at temperatures of 600 K and 903 K. The second objective addressed is the comprehensive characterization of three alloy compositions that were selected and elaborated, namely Bi25Sn75, Bi50Sn50, and Bi75Sn25, and morphological and structural investigations were carried out on them.

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The scope of this study consists of setting up of an integrated cost-effective sampling & laboratory analyses procedure which delineates sampling, sub-sampling and analytical uncertainties in case of fine-grained extractive waste deposits. This procedure is designed to support the decision makers towards fine-grained waste deposits upcycling and land reclamation. This procedure consists of a balanced replicated sampling design (BRSD) coupled with a three split levels ANOVA data processing.

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The β-Ti alloys have attracted the attention of researchers due to their excellent properties and their remarkable biocompatibility. The present study evaluated the mechanical behavior analysis (hardness, compressive strength, and modulus of elasticity) of the Ti-15Mo-W system. For experimental research, we chose the TiMo15 biocompatible alloy as a starting material.

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Increasing global lead consumption has been mainly supported by the acid battery manufacturing industry. As the lead demand will continue to grow, to provide the necessary lead will require an efficient approach to recycling lead acid batteries. In this paper was performed a mathematical modeling of the process parameters for lead recovery from spent lead-acid batteries.

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