This study presents a significant development in the Energy-Resolved Neutron Imaging System RADEN, in the Japan Proton Accelerator Research Complex, Japan. Through a systematic study, the collimation power of the facility was reevaluated. What was initially considered to be values of 230, 420, and 760 have been proven to be much higher.
View Article and Find Full Text PDFAmongst the more than 18 different forms of water ice, only the common hexagonal phase and the cubic phase are present in nature on Earth. Nonetheless, it is now widely recognized that all samples of 'cubic ice' discovered so far do not have a fully cubic crystal structure but instead are stacking-disordered forms of ice I (namely, ice Isd), which contain both hexagonal and cubic stacking sequences of hydrogen-bonded water molecules. Here, we describe a method to obtain large quantities of cubic ice Ic with high structural purity.
View Article and Find Full Text PDFDeuterated ice XVII, a metastable solid water polymorph, was filled with Ne and O2 at p ≈ 100 kPa and studied by in situ neutron diffraction (ILL, France). Powder patterns were collected in the ranges of 20-50 K (Ne) and 4.6-90 K (O2).
View Article and Find Full Text PDFExperimental tests are presented that assess the cross-talk level among three scintillation detectors used as neutron counters exploiting the thermal neutron radiative capture on Cd. The measurements were done at the INES diffractometer operating at the ISIS spallation neutron source (Rutherford Appleton Laboratory, UK). These tests follow a preliminary set of measurements performed on the same instrument to study the effectiveness of this thermal neutron counting strategy in neutron diffraction measurements, typically performed on INES using squashed He filled gas tubes.
View Article and Find Full Text PDFDistribution, penetration depth and amount of new mineralogical phases formed after the interaction between an inorganic treatment and a matrix are key factors for the evaluation of the conservation treatment behaviour. Nowadays, the conventional analytical methodologies, such as vibrational spectroscopies, scanning electron microscopy and X-ray diffraction, provide only qualitative and spot information. Here, we report, for the first time, the proof of concept of a methodology based on neutron imaging able to achieve quantitative data useful to assess the formation of calcium oxalate in a porous carbonatic stone treated with ammonium oxalate.
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