Development and validation of a multianalyte method for quantification of mycotoxins and pesticides in rice using a simple dilute and shoot procedure and UHPLC-MS/MS.

In the present manuscript an analytical methodology for the simultaneous determination of ten mycotoxins and six pesticides in rice was developed. This methodology comprises the application of the dilute and shoot protocol followed by quantification via UHPLC-MS/MS. The methodology was validated and all figures of merit shown to be within the limits established by regulation.