Evidence of the Monopolar-Dipolar Crossover Regime: A Multiscale Study of Ferroelastic Domains by In Situ Microscopy Techniques.

The elastic interaction between kinks (and antikinks) within domain walls plays a pivotal role in shaping the domain structure, and their dynamics. In bulk materials, kinks interact as elastic monopoles, dependent on the distance between walls (d) and typically characterized by a rigid and straight domain configuration. In this work the evolution of the domain structure is investigated, as the sample size decreases, by the means of in situ heating microscopy techniques on free-standing samples.

Acoustic emission of kidney stones: a medical adaptation of statistical breakdown mechanisms.

Kidney stones have a prevalence rate of > 10% in some countries. There has been a significant increase in surgery to treat kidney stones over the last 10 years, and it is crucial that such techniques are as effective as possible, while limiting complications. A selection of kidney stones with different chemical and structural properties were subjected to compression.

Crackling noise microscopy.

Crackling noise is a scale-invariant phenomenon found in various driven nonlinear dynamical material systems as a response to external stimuli such as force or external fields. Jerky material movements in the form of avalanches can span many orders of magnitude in size and follow universal scaling rules described by power laws. The concept was originally studied as Barkhausen noise in magnetic materials and now is used in diverse fields from earthquake research and building materials monitoring to fundamental research involving phase transitions and neural networks.

Avalanche criticality in LaAlO[Formula: see text] and the effect of aspect ratio.

Ferroic domain dynamics, as a function of external stimuli, can be collectively described as scale-invariant avalanches characterised by a critical exponent that are sensitive to the complexity of the domain microstructure. The understanding and manipulation of these avalanches lies at the heart of developing novel applications such as neuromorphic computing. Here we combine in situ heating optical observations and mean-field analysis to investigate the collective domain behaviour in pure-ferroelastic lanthanum aluminate (LaAlO[Formula: see text]) as a function of aspect ratio, the ratio of sample length to width, where the movement of the domains is predominantly driven by thermal stresses via thermal expansion/contraction during heat cycling.

Energy exponents of avalanches and Hausdorff dimensions of collapse patterns.

A simple numerical model to simulate athermal avalanches is presented. The model is inspired by the "porous collapse" process where the compression of porous materials generates collapse cascades, leading to power law distributed avalanches. The energy (E), amplitude (A_{max}), and size (S) exponents are derived by computer simulation in two approximations.

Cracking of human teeth: An avalanche and acoustic emission study.

Teeth are the hardest part of the human body. Cracking of human teeth under compression progresses by avalanches emitting acoustic noise. Acoustic emission (AE) spectroscopy reveals that tooth avalanches are statistically fully compatible with predictions of mean field (MF) theory.

Twisting of a Pristine α-Fe Nanowire: From Wild Dislocation Avalanches to Mild Local Amorphization.

The torsion of pristine α-Fe nanowires was studied by molecular dynamics simulations. Torsion-induced plastic deformation in pristine nanowires is divided into two regimes. Under weak torsion, plastic deformation leads to dislocation nucleation and propagation.

The duration-energy-size enigma for acoustic emission.

Acoustic emission (AE) measurements of avalanches in different systems, such as domain movements in ferroics or the collapse of voids in porous materials, cannot be compared with model predictions without a detailed analysis of the AE process. In particular, most AE experiments scale the avalanche energy E, maximum amplitude Amax and duration D as E ~ A and A ~ D with x = 2 and a poorly defined power law distribution for the duration. In contrast, simple mean field theory (MFT) predicts that x = 3 and χ = 2.

Avalanche criticality during ferroelectric/ferroelastic switching.

Field induced domain wall displacements define ferroelectric/ferroelastic hysteresis loops, which are at the core of piezoelectric, magnetoelectric and memristive devices. These collective displacements are scale invariant jumps with avalanche characteristics. Here, we analyse the spatial distribution of avalanches in ferroelectrics with different domain and transformation patterns: Pb(MgNb)O-PbTiO contains complex domains with needles and junction patterns, while BaTiO has parallel straight domains.

Domain Dynamics in Quantum-Paraelectric SrTiO_{3}.

Twin dynamics forced by acoustic waves shows several linear and nonlinear response modes below T_{c}=106  K. In the quantum paraelectric state a "quantum domain glass" at 25  K View Article and Find Full Text PDF

Ferroelectric switching in ferroelastic materials with rough surfaces.

Electric switching of non-polar bulk crystals is shown to occur when domain walls are polar in ferroelastic materials and when rough surfaces with steps on an atomic scale promote domain switching. All domains emerging from surface nuclei possess polar domain walls. The progression of domains is then driven by the interaction of the electric field with the polarity of domain boundaries.

Periodicity-Doubling Cascades: Direct Observation in Ferroelastic Materials.

Very sensitive responses to external forces are found near phase transitions. However, transition dynamics and preequilibrium phenomena are difficult to detect and control. We have observed that the equilibrium domain structure following a phase transition in ferroelectric and ferroelastic BaTiO_{3} is attained by halving of the domain periodicity multiple times.

Author Correction: Temperature Chaos, Memory Effect, and Domain Fluctuations in the Spiral Antiferromagnet Dy.

A correction to this article has been published and is linked from the HTML and PDF versions of this paper. The error has not been fixed in the paper.

Avalanche mixing and the simultaneous collapse of two media under uniaxial stress.

Avalanches in coal and sandstone samples under common uniaxial stress serve as a model for mixing of avalanche exponents in ceramics, multiferroics, and alloys. The two media are sandwiched together and subjected to common uniaxial stress using high- and low-stress compression. Each medium collapses individually through avalanches that often coincide with secondary avalanches into the other medium.

Temperature Chaos, Memory Effect, and Domain Fluctuations in the Spiral Antiferromagnet Dy.

The spiral antiferromagnetic phase of polycrystalline dysprosium between 140 K and the Néel temperature at 178 K and its domain wall (DW) dynamics were investigated using high-resolution ultrasonic spectroscopy. Two kinetic processes of quasi-static DW motion occur under non-isothermal and isothermal conditions. A "fast" process is proportional to the rate of the temperature change and results in a new category of anelastic phenomena: magnetic transient ultrasonic internal friction (IF).

Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars.

Compressed nano-pillars crackle from moving dislocations, which reduces plastic stability. Crackling noise is characterized by stress drops or strain bursts, which scale over a large region of sizes leading to power law statistics. Here we report that this "classic" behaviour is not valid in Ti-based nanopillars for a counterintuitive reason: we tailor precipitates inside the nano-pillar, which "regulate" the flux of dislocations.

Acoustic Emission from Porous Collapse and Moving Dislocations in Granular Mg-Ho Alloys under Compression and Tension.

We identified heterogeneous Mg-Ho alloys as an ideal material to measure the most extensive acoustic emission spectra available. Mg-Ho alloys are porous and show a high density of dislocations, which slide under external tension and compression. These dislocations nucleate near numerous heterogeneities.

Glasslike Dynamics of Polar Domain Walls in Cryogenic SrTiO_{3}.

Polar and highly mobile domain walls in SrTiO_{3} move under electric and elastic fields. Two vastly different timescales dominate their dynamical behavior. The previously observed fast changes lead to anomalies near 40 K where the elastic moduli soften and the polarity of the walls becomes strong.

Experimental Evidence of Accelerated Seismic Release without Critical Failure in Acoustic Emissions of Compressed Nanoporous Materials.

The total energy of acoustic emission (AE) events in externally stressed materials diverges when approaching macroscopic failure. Numerical and conceptual models explain this accelerated seismic release (ASR) as the approach to a critical point that coincides with ultimate failure. Here, we report ASR during soft uniaxial compression of three silica-based (SiO_{2}) nanoporous materials.

Analysis of crackling noise using the maximum-likelihood method: Power-law mixing and exponential damping.

Crackling noise can be initiated by competing or coexisting mechanisms. These mechanisms can combine to generate an approximate scale invariant distribution that contains two or more contributions. The overall distribution function can be analyzed, to a good approximation, using maximum-likelihood methods and assuming that it follows a power law although with nonuniversal exponents depending on a varying lower cutoff.

Locally preserved α → β phase transition in natural radiation-damaged titanite (CaTiSiO): evidence from laser-induced photoluminescence and dielectric measurements.

In situ temperature-dependent laser-induced photoluminescence and dielectric measurements provide new evidence for the local occurrence of the α  →  β phase transition near 500 K in the preserved crystalline parts of natural radiation-damaged titanite (sample E2335 with ~24% amorphous fraction, containing Fe and Al impurities). Photoluminescence spectroscopic measurements show an anomaly in the vicinity of 500 K. The temperature-dependent evolution of the real part of the electrical conductivity (σ) and the real (ε') and the imaginary (ε″) part of the complex dielectric permittivity (ε ) of titanite have been measured at various AC frequencies (~1.

Predicting mining collapse: Superjerks and the appearance of record-breaking events in coal as collapse precursors.

The quest for predictive indicators for the collapse of coal mines has led to a robust criterion from scale-model tests in the laboratory. Mechanical collapse under uniaxial stress forms avalanches with a power-law probability distribution function of radiated energy P∼E^{-}^{ɛ}, with exponent ɛ=1.5.

Imaging and tuning polarity at SrTiO domain walls.

Electrostatic fields tune the ground state of interfaces between complex oxide materials. Electronic properties, such as conductivity and superconductivity, can be tuned and then used to create and control circuit elements and gate-defined devices. Here we show that naturally occurring twin boundaries, with properties that are different from their surrounding bulk, can tune the LaAlO/SrTiO interface 2DEG at the nanoscale.

Avalanche criticality during compression of porcine cortical bone of different ages.

Crack events developed during uniaxial compression of cortical bones cut from femurs of developing pigs of several ages (4, 12, and 20 weeks) generate avalanches. These avalanches have been investigated by acoustic emission analysis techniques. The avalanche energies are power-law distributed over more than four decades.

Direct observation of polar tweed in LaAlO3.

Polar tweed was discovered in mechanically stressed LaAlO3. Local patches of strained material (diameter ca. 5 μm) form interwoven patterns seen in birefringence images, Piezo-Force Microscopy (PFM) and Resonant Piezoelectric Spectroscopy (RPS).