Three different magnetic samples with particle sizes ranging from 10 to 30 nm were prepared by wet chemical methods. The powders were heated at 100, 150, 200, and 250 °C during 30 min under air. Ferrous and total iron contents were determined immediately after the synthesis and after the thermal treatments.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
January 2013
The heterosite phase occurring in a pegmatitic rock sample was characterized by X-ray diffraction, by energy-dispersive X-ray spectroscopy and by Mössbauer spectroscopy. The orthorhombic unit-cell parameters, expressed in Å, were found as a=9.733 (1), b=5.
View Article and Find Full Text PDFA detailed 57Fe Mössbauer study of the Mg(0.8)Fe(0.2-y)Co(y)Al2O4 (y = 0, 0.
View Article and Find Full Text PDFMg(0.90)Fe(x)Co(y)O (x + y = 0.1) solid solutions were synthesized by the ureic combustion route.
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