Publications by authors named "Earl J Kirkland"

Aberration correctors offer greatly enhanced resolution in electron microscopes, however can require dramatically more complicated adjustments. A method of computer adjustment of a probe forming aberration corrector in a Scanning Transmission Electron Microscope (STEM) is proposed and analyzed using image simulation. This method works directly with the image and should work well with crystalline specimens.

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Computation in electron microscopy.

Acta Crystallogr A Found Adv

January 2016

Some uses of the computer and computation in high-resolution transmission electron microscopy are reviewed. The theory of image calculation using Bloch wave and multislice methods with and without aberration correction is reviewed and some applications are discussed. The inverse problem of reconstructing the specimen structure from an experimentally measured electron microscope image is discussed.

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New aberration correctors present new challenges in optimizing (minimizing) the probe size in the STEM (Scanning Transmission Electron Microscope). A small probe is important for high resolution imaging and analytical microscopy. Some effects of aperture size, corrector accuracy, and higher order aberrations on probe size and image artifacts are calculated.

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Article Synopsis
  • Aberration correctors address optical flaws, but they don't fix issues caused by environmental instabilities.
  • Improved spatial resolution in microscopes makes them more sensitive to surrounding factors, meaning room design is crucial for optimal performance.
  • The text explores ways to measure and understand how various environmental disturbances affect microscope imaging and spectroscopy, highlighting the limitations these factors impose.
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As an electron beam (of order 100 keV) travels through a crystalline solid it can be channeled down a zone axis of the crystal to form a channeling peak centered on the atomic columns. The channeling peak can be similar in size to the outer atomic orbitals. Electron energy loss spectroscopy (EELS) measures the losses that the electron experiences as it passes through the solid yielding information about the unoccupied density of states in the solid.

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