This work is devoted to magnesium oxide (MgO) nanoparticles (NPs) for their use as additives for bone implants. Extracts from four different widely used plants, including , , , and , were evaluated for their ability to facilitate the "green synthesis" of MgO nanoparticles. The thermal stability and decomposition behavior of the MgONPs were analyzed by thermogravimetric analysis (TGA).
View Article and Find Full Text PDFEarly detection of diseases can increase the chances of successful treatment and survival. Therefore, it is necessary to develop a method for detecting or sensing biomolecules that cause trouble in living organisms. Disease sensors should possess specific properties, such as selectivity, reproducibility, stability, sensitivity, and morphology, for their routine application in medical diagnosis and treatment.
View Article and Find Full Text PDFHere, surface-enhanced Raman scattering (SERS) and tip-enhanced Raman scattering (TERS) were used to characterize the selective adsorption of N-substituted 4-[(NH-R)(phosphono)-S-methyl]phenylboronic acids on the surface of platinum nanoparticles (PtNPs) from an aqueous solution and from air. The nature of the interaction of the studied compounds with the PtNPs/H O and PtNPs/air interfaces was discussed and compared. For this purpose, 4-[(N-anilino)(phosphono)-S-methyl]phenylboronic acid (1-PBA-PA) and its two analogs (2-PBA-PA and bis{1-PBA-PA}) as well as the PtNPs were synthesized in surfactant/ion-free solution via a synthetic route that allows control of the size and morphology of the NPs.
View Article and Find Full Text PDFSpectrochim Acta A Mol Biomol Spectrosc
March 2023
This work describes biologically important nanostructures of metals (AgNPs, AuNPs, and PtNPs) and metal oxides (CuONPs, CuONSs, γ-FeONPs, ZnONPs, ZnONPs-GS, anatase-TiONPs, and rutile-TiONPs) synthesized by different methods (wet-chemical, electrochemical, and green-chemistry methods). The nanostructures were characterized by molecular spectroscopic methods, including scanning/transmission electron microscopy (SEM/TEM), energy dispersive X-ray spectroscopy (EDS), X-ray diffraction analysis (XRD), photoelectron spectroscopy (XPS), ultraviolet-visible spectroscopy (UV-vis), dynamic light scattering (DLS), Raman scattering spectroscopy (RS), and infrared light spectroscopy (IR). Then, a peptide (bombesin, BN) was adsorbed onto the surface of these nanostructures from an aqueous solution with pH of 7 that did not contain surfactants.
View Article and Find Full Text PDFEleven multiple analogs of bradykinin-a peptide that is a natural ligand of B1 and B2 receptors but does not bind or activate the B1 receptor unless Arg is removed from the sequence by the action of carboxypeptidase N-were synthesized. Their biological activity was examined on T-REx cell lines expressing B1 or B2 receptors using the intracellular IP1 assay. The mRNA expression of B1R and B2R in the lysate of tumor cell lines, e.
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