Introduction: The association between motor capacity and the level of disability in patients with fibromyalgia remains underexplored. This study aims to explore the association between physical capacity tests explored in the consultation and the level of disability in women with fibromyalgia.
Methods: There were 484 women diagnosed with fibromyalgia who were evaluated with 7 physical capacity tests: 10-m walk, 2-minute walk, 5-repetition getting up from a chair and sitting (G&S), 30-second chair stand, monopodal balance (right and left), and up-and-go.
Herein, the effectiveness of an itaconic acid (IA) graft copolymer on native corn starch (NCS) as a filter control agent in fresh water-based drilling fluids (WBDFs) was evaluated. The copolymer (S--IA_APS) was synthesized by conventional radical dispersion polymerization using the redox initiation system (NH)SO/NaHSO. The modification of the starches was verified by volumetry, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM).
View Article and Find Full Text PDFMaterials (Basel)
October 2019
Superabsorbents starches (SASs) were synthesized and characterized starting from native corn starch, bitter cassava and sweet cassava by graft copolymerization with itaconic acid. Additionally, their swelling behavior was studied both in water and in buffer solutions with different pHs and saline solutions. Their applicability was tested as environmentally friendly fertilizers in the absorption and release of urea, potassium nitrate and ammonium nitrate at different concentrations of fertilizers.
View Article and Find Full Text PDFHerein, hydrogels based on starch from corn, sweet cassava and bitter cassava were prepared by a straightforward approach. The hydrogels were obtained by an oxidation process using the redox system KMnO/NaHSO which leads to the formation of carbonyl and carboxyl groups with minimum polymer hydrolysis. The resulting oxidized samples as well as the native starches were extensively characterized by scanning electron microscopy, thermogravimetric analysis and wide angle X-ray scattering, among others.
View Article and Find Full Text PDFDifferent oxidized chitosans were prepared following various approaches, by thermo-acid oxidation or by using KMnO/NaHSO, (NH)SO/NaHSO and KCrO/NaHSO redox pairs added sequentially or simultaneously. All these reactions pursue the formation of carboxylic groups which enhance their capability to remove model cationic and anionic dyes such as methylene blue and methyl orange, respectively. The resulting oxidized chitosans were structurally and thermally characterized by elemental analysis, infrared spectroscopy, nuclear magnetic resonance, scanning electron microscopy and thermogravimetry.
View Article and Find Full Text PDFActa Crystallogr Sect E Struct Rep Online
October 2013
In the title compound, C21H22N2O, the planes of the two six-membered rings make a dihedral angle of 89.51 (7)°. The pyrrolidine ring has a puckering amplitude q 2 = 0.
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