The purpose of this study was synthesis of photoluminescent nanoparticles for detection of toxic metal ions. Also, these controllable magnetic nanocomposites were used for detection of bacteria. Carbon nano-templates were formed by calcination and sonication of lemon extract as a bio-compatible precursor.
View Article and Find Full Text PDFMagnetic-plasmonic nanocomposites are suitable candidates for photocatalytic activity due to both optical and magnetic properties. So initially, we synthesized strontium hexaferrite nanoparticles (NPs) by three different methods: microwave, sol-gel Pechini, sol-gel auto-combustion, and SrFeO@Ag, SrFeO@Au core-shell by ultrasound-assisted auto-combustion in the presence of beetroot juice. X-Ray Powder Diffraction (XRD), Fourier Transform Infrared (FT-IR), Energy Dispersive X-Ray (EDX), Field Emission Scanning Electron Microscopy (FE-SEM), Transmission Electron Microscopy (TEM), Brunauer-Emmett-Teller (BET), Diffuse Reflectance Spectroscopy (DRS), and Vibrating Sample Magnetometer (VSM) analyses were utilized to examine their purity, morphology, optical and magnetic properties.
View Article and Find Full Text PDFThe aim of this work is synthesis of magnetic and photoluminescence (PL) nano-fibers for detection of mercury (II) and lead (II) ions that are toxic and their detection are necessary. Prepared nanoparticles are controllable by external magnetic field, so their threat is much lesser than non-magnetic material. Firstly, iron nanoparticles were achieved with ball milling procedure and cellulose acetate (CA) nano-fibers were prepared by electro spinning procedure.
View Article and Find Full Text PDFIn the present research, a novel kind of homogeneous cation-exchange membranes were provided by solution casting technique via blending of sulfonated polyvinylchloride (SPVC) and sulfonated poly phenylene oxide (SPPO). The performance of the membranes was evaluated by membrane potential, areal resistance, transport number, ionic permeability, ion-exchange capacity, fixed ion concentration, energy consumption (EC), current efficiency, mechanical properties, membrane oxidative stability, water contact angle and water content tests. The microstructures of the membranes were investigated by scanning electron microscopy.
View Article and Find Full Text PDFThe aim of this work is preparing of a photoluminescence nanostructures for rapid detection of bacterial pathogens. Firstly, carbon dots (CDs) were synthesized by grape fruit, lemon, turmeric extracts and hydrothermal method. Then FeO (magnetite) nanoparticles was achieved using these bio-compatible capping agents.
View Article and Find Full Text PDFIn this work, copper pyrovanadate (Cu3V2O7(OH)2(H2O)2) nanoparticles have been synthesized by a simple and rapid chemical precipitation method. Different copper-organic complexes were used to control the size and morphology of products. The morphology and structure of the as-synthesized products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectrum, electron dispersive X-ray spectroscopy (EDX), thermal gravimetric analysis (TGA), differential thermal analysis (DTA) and photoluminescence (PL) spectroscopy.
View Article and Find Full Text PDFDifferent morphologies of Ag2Te nanostructures were synthesized using TeCl4 as a new precursor and hydrazine hydrate as reducing agent by a hydrothermal method. Various parameters that affect on morphology and purity of nanostructures were optimized. According to our experiments the best time and temperature for preparation of this nanostructure are 12 h and 120 °C.
View Article and Find Full Text PDFComb Chem High Throughput Screen
February 2014
In this paper, CuInS2 (CIS) nanoparticles were synthesized successfully via a new copper precursor [bis(acetylacetonato)copper(II)], [Cu(acac)2]; at room temperature by ultrasonic method. The effect of sulfur source, solvent, and reaction time was investigated on product morphology and particle size. A series of analyses was performed to characterize the CuInS2 microsphere including X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and photoluminescence (PL) spectroscopy.
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