This study investigated the homogeneous synthesis of cellulose acetate (CA) and propionate (CP) with varying degrees of substitution (DS) from sisal cellulose in a N, N-dimethylacetamide/lithium chloride (DMAc/LiCl) solvent system. These esters were used to prepare neat (CAF/CPF) and nanocomposite films (CAFFe/CPFFe) from prior synthesized magnetite nanoparticles (NPs, FeO, 5.1 ± 0.
View Article and Find Full Text PDFChemical precursors for nanomaterials synthesis have become essential to tune particle size, composition, morphology, and unique properties. New inexpensive precursors investigation that precisely controls these characteristics is highly relevant. We studied new Se precursors, the acid selenites (R-O-SeOOH), to synthesize CdSe quantum dots (QDs).
View Article and Find Full Text PDFAtmospheric particulate material (PM) from mining and steel industries comprises several metallic contaminants. PM samples collected in a Brazilian region with a recognized influence of the steel and iron pelletizing industries were used to investigate metallic nanoparticle incorporation into human fibroblast cells (MRC-5). MRC-5 cells were exposed to 0 (control, ultrapure water), 2.
View Article and Find Full Text PDFTadpole-like gold nanowires were obtained by the oleylamine-mediated synthesis presenting an unusual mixture of fcc and hcp phases. Structural analyses were performed to understand their structure and growth using aberration-corrected high-resolution scanning transmission electron microscopy and electron diffraction at the tail region of tadpoles showing that the anisotropic shape occurred due to stacking fault defects. Stacking faults and twin defects are responsible for the hcp phase inferring a defect dependent growth.
View Article and Find Full Text PDFFecal samples from 27 pigs were longitudinally analyzed for Teschovirus A (TV-A), Sapelovirus A (SV-A), and Enterovirus G (EV-G) RNA presence. Suckling piglet fecal samples were negative for the three enteric picornaviruses. However, these picornaviruses were detected in 22/27 weaned pig fecal samples.
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