The identification and recovery of suspected human biofluid evidence can present a bottleneck in the crime scene investigation workflow. Crime Scene Investigators typically deploy one of a number of presumptive enhancement reagents, depending on what they perceive an analyte to be; the selection of this reagent is largely based on the context of suspected evidence and their professional experience. Positively identified samples are then recovered to a forensic laboratory where confirmatory testing is carried out by large lab-based instruments, such as through mass-spectrometry-based techniques.
View Article and Find Full Text PDFPhotometric Stereo and Elastomeric Sensor Imaging were assessed for measuring the 3-dimensional (3D) morphology of questioned document samples. Photometric stereo is shown to be a powerful non-contact technique for revealing micron level detail of the samples examined. Elastomeric Sensor Imaging is shown to complement photometric stereo by yielding equivalent results.
View Article and Find Full Text PDFJ Mech Behav Biomed Mater
December 2022
Regional mechanics of skeletal muscle were investigated from equibiaxial testing in vitro on tissue samples. Samples were collected in three excising zones in transversal direction to the myofibers. Thus, the transverse plane stiffness, likely to be dictated by extracellular matrix collagen (ECM), was studied.
View Article and Find Full Text PDFThe identification of individuals, particularly at international border crossings, coupled with the evolving sophistication of identity documents are issues that authorities must contend with. Particularly, the ability to distinguish legitimate from counterfeit documents, with high throughput, sensitivity, and selectivity is an ever-evolving challenge. Over the last decade, an increasing number of security features have been introduced by authorities in identification documents.
View Article and Find Full Text PDFBromine has been added to cis,trans,trans-1,5,9-cyclododecatriene under various reaction conditions. All expected direct addition products have been isolated, and their structures have been determined by microanalysis, NMR and X-ray crystallography. Advanced NMR techniques were used to determine solution conformations of several of the compounds, enabling comparison with the solid-state conformations obtained by crystallography.
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