Layered zinc(II) hydroxides (LZH) intercalating the deprotonated forms of -(-) or -(+)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate (denoted as - or -BNDHPH, respectively) were prepared from Zn(NO) at pH 5 and 60 °C by the mixing method. The obtained hybrid compounds (denoted as - or -BNDHP/LZH, respectively) were heated from room temperature up to 800 °C under nitrogen atmosphere. According to the thermal gravimetric/differential thermal analysis measurements, hydroxyl groups were dehydrated at 270-400 °C, followed by the decomposition of organic components at 420-600 °C.
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