Ultraperformance liquid chromatography (UPLC) and ion mobility (IM) spectrometry were interfaced with mass spectrometry (MS) and tandem mass spectrometry (MS/MS) to characterize a complex nonionic surfactant mixture. The surfactant was composed of a glycerol core, functionalized with poly(ethylene oxide) units (PEO) that were partially esterified by caprylic and/or capric acid. Reversed-phase UPLC classified the blend based on polarity into four groups of eluates, corresponding to compounds with zero, one, two, or three fatty acid residues.
View Article and Find Full Text PDFThis study evaluated the aerobic demands of the 20-minute steady-state jogging speeds for 15 high school students. All subjects performed a discontinuous treadmill test that included submaximal speeds, the Fit Youth Today criterion referenced speeds, and finally a run to voluntary fatigue. Stages lasted 5 minutes.
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