In situ Fe-doped thin carbon wires via AC high voltage arc discharge.

This study explores the controlled, continuous production of thin carbon rods between graphite electrodes (continued electrode deposits) during an arc discharge of high voltage alternating current with a frequency of 50 Hz in liquid paraffin, along with in situ doping of the resulting material using a suspension of liquid paraffin and iron powder ( <10 μm). The surface morphology of the obtained carbon rod nanomaterials was characterized using scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX), scanning transmission electron microscopy (STEM) with EDX chemical composition analysis, X-ray microtomography (micro-CT), and atomic force microscopy (AFM). The AFM technique in scanning thermal microscopy (SThM) and conductive probe (CP) modes was employed to determine the temperature and electrical conductivity of the obtained nanostructures.

Correction: Naked and necked gold nanoparticles prepared by submerged alternating current arc discharge in water.

[This corrects the article DOI: 10.1039/D2RA06050G.].

Necked gold nanoparticles prepared by submerged alternating current arc discharge in water.

The article presents the method of producing gold nanoparticles using a high voltage arc discharge of alternating current with a frequency of 50 Hz in distilled water. The equipment necessary to carry out the process is described, including the construction of the reactor and the power source of a very simple design necessary to generate a high-voltage arc discharge between the electrodes. Arc discharge processes were carried out two times for 2 and 5 minutes, respectively, in ambient conditions without thermostating the reactor, at medium temperature varying in the range of 25-70 °C.